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@ARTICLE{Mahr:893899,
author = {Mahr, Christoph and Müller-Caspary, Knut and Ritz, Robert
and Simson, Martin and Grieb, Tim and Schowalter, Marco and
Krause, Florian and Lackmann, Anastasia and Soltau, Heike
and Wittstock, Arne and Rosenauer, Andreas},
title = {{I}nfluence of distortions of recorded diffraction patterns
on strain analysis by nano-beam electron diffraction},
journal = {Ultramicroscopy},
volume = {196},
issn = {0304-3991},
address = {Amsterdam},
publisher = {Elsevier Science},
reportid = {FZJ-2021-02911},
pages = {74 - 82},
year = {2019},
abstract = {Images acquired in transmission electron microscopes can be
distorted for various reasons such as e.g. aberrations of
the lenses of the imaging system or inaccuracies of the
image recording system. This results in inaccuracies of
measures obtained from the distorted images. Here we report
on measurement and correction of elliptical distortions of
diffraction patterns. The effect of this correction on the
measurement of crystal lattice strain is investigated. We
show that the effect of the distortions is smaller than the
precision of the measurement in cases where the strain is
obtained from shifts of diffracted discs with respect to
their positions in images acquired in an unstrained
reference area of the sample. This can be explained by the
fact that diffraction patterns acquired in the strain free
reference area of the sample are distorted in the same
manner as the diffraction patterns acquired in the strained
region of interest. In contrast, for samples without a
strain free reference region such as nanoparticles or
nanoporous structures, where we evaluate ratios of lattice
plane distances along different directions, the distortions
are usually not negligible. Furthermore, two techniques for
the detection of diffraction disc positions are compared
showing that for samples in which the crystal orientation
changes over the investigated area it is more precise to
detect the positions of many diffraction discs
simultaneously instead of detecting each disc position
independently.},
cin = {ER-C-1},
ddc = {570},
cid = {I:(DE-Juel1)ER-C-1-20170209},
pnm = {5351 - Platform for Correlative, In Situ and Operando
Characterization (POF4-535) / moreSTEM - Momentum-resolved
Scanning Transmission Electron Microscopy (VH-NG-1317)},
pid = {G:(DE-HGF)POF4-5351 / G:(DE-HGF)VH-NG-1317},
typ = {PUB:(DE-HGF)16},
pubmed = {30291992},
UT = {WOS:000451180800011},
doi = {10.1016/j.ultramic.2018.09.010},
url = {https://juser.fz-juelich.de/record/893899},
}