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@INPROCEEDINGS{Nandakumaran:894053,
author = {Nandakumaran, N. and Feygenson, M. and Fanatechi, E. and
Pinieder, F. and Feoktystov, Artem and Brückel, Thomas},
title = {{I}nvestigating self-assembly of {A}u-{F}e3{O}4 dumbbell
nanoparticles using advanced scattering techniques},
reportid = {FZJ-2021-03007},
year = {2021},
abstract = {We investigated parameters that affect self-assembly of
magnetic dumbbellnanoparticles (DBNPs) in solution. The
dumbbells consist of epitaxially grownmagnetic Fe3O4
nanoparticles on the surface of spherical Au nanoparticles.
Theirstructural, optical and magnetic properties are useful
for variety of applications suchas dual probes for drug
delivery [1-2], catalysis [3], sensing [4], optics [5]
andelectronics [6]. However, fundamental understanding of
mechanisms and parametersinvolved in self-assembly of DBNPs
in solution is still missing. We studied severalDBNPs coated
with a mixture of oleic acid and oleylamine of different
sizes: A13F14,A11F8, A10F14, A10F12, A9F11, where numbers
indicate the diameters of Au (A)and Fe3O4 (F), respectively.
Field-dependent DC magnetization reveals differentshapes of
hysteresis loops for our samples, which is presumably due to
a Au/Fe3O4interface and modification of magnetization
profile of Fe3O4 [7-8]. Small-angle neutronscattering in
applied magnetic field showed self-assembly of DBNPs in
solutions, incontrast to zero-field measurements. We
observed the onset of order beginning at0.2 T for A10F14,
A9F11 and at 1T for A13F14 (Figure 1). Surprisingly, we
found noself-assembly for A10F12 and A11F8 even at 3T. We
also performed a polarizedSANS at 1T and 3T to separate
nuclear and weak magnetic scattering.},
month = {May},
date = {2021-05-31},
organization = {725. WE-Heraeus-Seminar: Magnetic
Small Angle Neutron Scattering – from
Nanoscale Magnetism to Long‐Range
Magnetic Structures, online event
(online event), 31 May 2021 - 3 Jun
2021},
cin = {JCNS-2 / PGI-4 / JARA-FIT / JCNS-ESS / JCNS-FRM-II},
cid = {I:(DE-Juel1)JCNS-2-20110106 / I:(DE-Juel1)PGI-4-20110106 /
$I:(DE-82)080009_20140620$ / I:(DE-Juel1)JCNS-ESS-20170404 /
I:(DE-Juel1)JCNS-FRM-II-20110218},
pnm = {632 - Materials – Quantum, Complex and Functional
Materials (POF4-632) / 6G4 - Jülich Centre for Neutron
Research (JCNS) (FZJ) (POF4-6G4)},
pid = {G:(DE-HGF)POF4-632 / G:(DE-HGF)POF4-6G4},
typ = {PUB:(DE-HGF)1},
url = {https://juser.fz-juelich.de/record/894053},
}