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@ARTICLE{Lin:894219,
author = {Lin, Jingjing and Willbold, Sabine and Zinkevich, Tatiana
and Indris, Sylvio and Korte, Carsten},
title = {{I}onic ({P}roton) transport and molecular interaction of
ionic {L}iquid–{PBI} blends for the use as electrolyte
membranes},
journal = {Journal of molecular liquids},
volume = {342},
issn = {0167-7322},
address = {New York, NY [u.a.]},
publisher = {Elsevier},
reportid = {FZJ-2021-03108},
pages = {116964},
year = {2021},
abstract = {Protic ionic liquids (PILs) are discussed as new candidates
for the use as non-aqueous electrolytes for fuel cells
operating at temperatures above 80 °C. The molecular
interactions in Diethylmethylammonium triflate ([Dema][TfO])
doped polybenzimidazole (PBI) blend membranes and the proton
transport mechanism were investigated by means of TGA, IR
and NMR. The mobility of the PIL ions is restricted to the
PBI host polymer. The [Dema]+ cations and [TfO]− anions
interact strongly via H bonds with the polar groups of the
PBI chains. This will significantly confine the proton
conductivity of the membrane to vehicular transport. The
proton transport was investigated by comparing to an
analogous liquid state model using the monomer benzimidazole
(BIm) instead of the PBI polymer. During fuel cell
operation, it is unavoidable that residual water is present
in significant quantities. Resulting from 1H NMR and PFG
self-diffusion measurements, proton transport in the liquid
state model takes place via a cooperative mechanism
involving all of the species NH[Dema]+/NHBIm/H2O depending
on the water fraction. Thus, it is suggested that
conductivity in the PIL–PBI membrane be mainly provided by
the cooperative transport of the protons. This study is
intended to broaden understanding of the structure and
proton transport mechanism, as well as to give possible ways
to optimize PIL electrolyte doped polymer blend membranes
for intermediate operating temperatures.},
cin = {ZEA-3 / IEK-14},
ddc = {540},
cid = {I:(DE-Juel1)ZEA-3-20090406 / I:(DE-Juel1)IEK-14-20191129},
pnm = {1231 - Electrochemistry for Hydrogen (POF4-123)},
pid = {G:(DE-HGF)POF4-1231},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000708689300025},
doi = {10.1016/j.molliq.2021.116964},
url = {https://juser.fz-juelich.de/record/894219},
}