000894987 001__ 894987 000894987 005__ 20240712112813.0 000894987 0247_ $$2doi$$a10.1002/aesr.202100121 000894987 0247_ $$2Handle$$a2128/29372 000894987 0247_ $$2pmid$$aWOS:000783865000013 000894987 0247_ $$2WOS$$aWOS:000783865000013 000894987 037__ $$aFZJ-2021-03515 000894987 082__ $$a333.7 000894987 1001_ $$0P:(DE-Juel1)179011$$aSzczuka, Conrad$$b0$$eCorresponding author 000894987 245__ $$aIdentification of LiPF 6 Decomposition Products in Li‐Ion Batteries with Endogenous Vanadyl Sensors Using Pulse Electron Paramagnetic Resonance and Density Functional Theory 000894987 260__ $$aWeinheim$$bWiley-VCH$$c2021 000894987 3367_ $$2DRIVER$$aarticle 000894987 3367_ $$2DataCite$$aOutput Types/Journal article 000894987 3367_ $$0PUB:(DE-HGF)16$$2PUB:(DE-HGF)$$aJournal Article$$bjournal$$mjournal$$s1715084348_30445 000894987 3367_ $$2BibTeX$$aARTICLE 000894987 3367_ $$2ORCID$$aJOURNAL_ARTICLE 000894987 3367_ $$00$$2EndNote$$aJournal Article 000894987 520__ $$aThe evaluation and enhancement of Li-ion battery chemistries relies on detailed knowledge of the chemical processes occurring. Undesired side reactions have to be identified and correlated with used materials and operation/storage conditions, which requires suitable analytical tools, especially for minor and reactive species. Herein, a complementing experimental and theoretical method based on pulse electron paramagnetic resonance and density functional theory is presented using vanadyl ions as sensors for the chemical battery environment. The sensor is endogenously formed via cathode dissolution during battery operation. Probing the ligand sphere of the sensor, decomposition products of the electrolyte salt LiPF6 are identified, which are proposed to comprise P(+V) and P(+III) constituents. Extensive conformational flexibility of the ligands is observed, which is investigated in terms of structural parameters and holistically with molecular dynamics simulations. 000894987 536__ $$0G:(DE-HGF)POF4-1223$$a1223 - Batteries in Application (POF4-122)$$cPOF4-122$$fPOF IV$$x0 000894987 588__ $$aDataset connected to CrossRef, Journals: juser.fz-juelich.de 000894987 7001_ $$0P:(DE-Juel1)156296$$aJakes, Peter$$b1$$ufzj 000894987 7001_ $$0P:(DE-Juel1)156123$$aEichel, Rüdiger-A.$$b2 000894987 7001_ $$0P:(DE-Juel1)162401$$aGranwehr, Josef$$b3$$ufzj 000894987 773__ $$0PERI:(DE-600)3010017-3$$a10.1002/aesr.202100121$$gp. 2100121 -$$n12$$p210012$$tAdvanced energy & sustainability research$$v2$$x2699-9412$$y2021 000894987 8564_ $$uhttps://juser.fz-juelich.de/record/894987/files/aesr.202100121.pdf$$yOpenAccess 000894987 909CO $$ooai:juser.fz-juelich.de:894987$$pdnbdelivery$$pdriver$$pVDB$$popen_access$$popenaire 000894987 9101_ $$0I:(DE-588b)5008462-8$$6P:(DE-Juel1)179011$$aForschungszentrum Jülich$$b0$$kFZJ 000894987 9101_ $$0I:(DE-588b)5008462-8$$6P:(DE-Juel1)156296$$aForschungszentrum Jülich$$b1$$kFZJ 000894987 9101_ $$0I:(DE-588b)5008462-8$$6P:(DE-Juel1)156123$$aForschungszentrum Jülich$$b2$$kFZJ 000894987 9101_ $$0I:(DE-588b)36225-6$$6P:(DE-Juel1)156123$$aRWTH Aachen$$b2$$kRWTH 000894987 9101_ $$0I:(DE-588b)5008462-8$$6P:(DE-Juel1)162401$$aForschungszentrum Jülich$$b3$$kFZJ 000894987 9101_ $$0I:(DE-588b)36225-6$$6P:(DE-Juel1)162401$$aRWTH Aachen$$b3$$kRWTH 000894987 9131_ $$0G:(DE-HGF)POF4-122$$1G:(DE-HGF)POF4-120$$2G:(DE-HGF)POF4-100$$3G:(DE-HGF)POF4$$4G:(DE-HGF)POF$$9G:(DE-HGF)POF4-1223$$aDE-HGF$$bForschungsbereich Energie$$lMaterialien und Technologien für die Energiewende (MTET)$$vElektrochemische Energiespeicherung$$x0 000894987 9141_ $$y2021 000894987 915__ $$0StatID:(DE-HGF)0510$$2StatID$$aOpenAccess 000894987 915__ $$0LIC:(DE-HGF)CCBY4$$2HGFVOC$$aCreative Commons Attribution CC BY 4.0 000894987 915__ $$0StatID:(DE-HGF)0100$$2StatID$$aJCR$$bADV ENERG SUST RES : 2022$$d2023-08-28 000894987 915__ $$0StatID:(DE-HGF)0501$$2StatID$$aDBCoverage$$bDOAJ Seal$$d2021-09-30T11:01:43Z 000894987 915__ $$0StatID:(DE-HGF)0500$$2StatID$$aDBCoverage$$bDOAJ$$d2021-09-30T11:01:43Z 000894987 915__ $$0StatID:(DE-HGF)0030$$2StatID$$aPeer Review$$bDOAJ : Anonymous peer review$$d2021-09-30T11:01:43Z 000894987 915__ $$0LIC:(DE-HGF)CCBYNV$$2V:(DE-HGF)$$aCreative Commons Attribution CC BY (No Version)$$bDOAJ$$d2021-09-30T11:01:43Z 000894987 915__ $$0StatID:(DE-HGF)0199$$2StatID$$aDBCoverage$$bClarivate Analytics Master Journal List$$d2023-08-28 000894987 915__ $$0StatID:(DE-HGF)0112$$2StatID$$aWoS$$bEmerging Sources Citation Index$$d2023-08-28 000894987 915__ $$0StatID:(DE-HGF)0150$$2StatID$$aDBCoverage$$bWeb of Science Core Collection$$d2023-08-28 000894987 915__ $$0StatID:(DE-HGF)9905$$2StatID$$aIF >= 5$$bADV ENERG SUST RES : 2022$$d2023-08-28 000894987 915__ $$0StatID:(DE-HGF)0561$$2StatID$$aArticle Processing Charges$$d2023-08-28 000894987 915__ $$0StatID:(DE-HGF)0700$$2StatID$$aFees$$d2023-08-28 000894987 920__ $$lyes 000894987 9201_ $$0I:(DE-Juel1)IEK-9-20110218$$kIEK-9$$lGrundlagen der Elektrochemie$$x0 000894987 9801_ $$aFullTexts 000894987 980__ $$ajournal 000894987 980__ $$aVDB 000894987 980__ $$aI:(DE-Juel1)IEK-9-20110218 000894987 980__ $$aUNRESTRICTED 000894987 981__ $$aI:(DE-Juel1)IET-1-20110218