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@ARTICLE{Ye:897254,
author = {Ye, Ruijie and Ihrig, Martin and Imanishi, Nobuyuki and
Finsterbusch, Martin and Figgemeier, Egbert},
title = {{A} {R}eview on {L}i + /{H} + {E}xchange in {G}arnet
{S}olid {E}lectrolytes: {F}rom {I}nstability against
{H}umidity to {S}ustainable {P}rocessing in {W}ater},
journal = {ChemSusChem},
volume = {14},
number = {20},
issn = {1864-564X},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {FZJ-2021-03716},
pages = {4397-4407},
year = {2021},
abstract = {Garnet-based Li-ion conductors are one of the most
promising oxide-ceramic solid electrolytes for
next-generation Li batteries. However, they undergo a Li+/H+
exchange (LHX) reaction with most protic solvents used in
component manufacturing routes and even with moisture in
ambient air. These protonated garnets show a lower Li-ionic
conductivity, and even if only the surface is protonated,
this degraded layer hinders the Li-ion exchange with, for
example, a metallic Li anode. Furthermore, the resulting
unstable surface properties during the processing in air
lead to challenges with respect to reproducibility of the
final component performance, limiting their commercial
applicability. However, in recent years, the knowledge about
the underlying chemical mechanisms has led to the
development of mitigation strategies and enabled a push of
this promising material class towards sustainable and
scalable fabrication routes. This Minireview covers the
following four aspects, which are relevant for a
comprehensive understanding of these developments: (1)
reports of LHX phenomenon in garnets exposed to air and
solvents; (2) recent understandings of the fundamentals and
properties of LHX; (3) strategies to prevent LHX and to
recover garnets; and (4) sustainable application of LHX for
material processing and energy-related devices.},
cin = {IEK-1},
ddc = {540},
cid = {I:(DE-Juel1)IEK-1-20101013},
pnm = {1122 - Design, Operation and Digitalization of the Future
Energy Grids (POF4-112)},
pid = {G:(DE-HGF)POF4-1122},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:34264021},
UT = {WOS:000681376500001},
doi = {10.1002/cssc.202101178},
url = {https://juser.fz-juelich.de/record/897254},
}