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@ARTICLE{Deibert:902340,
      author       = {Deibert, Wendelin and Ivanova, Mariya E. and Huang, Yuanye
                      and Merkle, Rotraut and Maier, Joachim and Meulenberg,
                      Wilhelm A.},
      title        = {{F}abrication of multi-layered structures for proton
                      conducting ceramic cells},
      journal      = {Journal of materials chemistry / A},
      volume       = {10},
      issn         = {2050-7496},
      address      = {London ˜[u.a.]œ},
      publisher    = {RSC},
      reportid     = {FZJ-2021-04189},
      pages        = {2362-2373},
      year         = {2022},
      abstract     = {Protonic ceramic fuel cells offer a high potential to
                      produce electrical energy in a very efficient way. The
                      performance of such a device among others is highly
                      dependent on the electrolyte material and its thickness.
                      Therefore, multilayer structures are used to reduce the
                      electrolyte thickness down to 10–20 μm, supported by a
                      much thicker porous anode. In this work sequential
                      tape-casting is used to fabricate half-cells consisting of a
                      BZCY electrolyte and a BZCY/NiO support which also serves as
                      the anode layer. The starting powders are characterised as
                      well as the thermal behaviour of the half-cells during heat
                      treatment. Sintering experiments show that a temperature of
                      T ≥ 1450 °C is needed to achieve the desired
                      microstructure. After that a scale-up approach to a size of
                      the half-cells of about 25 cm2 is shown. The influence of
                      the processing temperature on the microstructure is shown by
                      detailed XRD and SEM studies. The formation of a BaY2NiO5
                      transient liquid phase during the heat treatment of the
                      cells is clearly demonstrated. Finally, the proton
                      conductivity of the tape-cast cells shows competitive values
                      of σ = 0.003 S cm−1 at 600 °C with the advantage of an
                      industrially proven and up-scalable manufacturing
                      technique.},
      cin          = {IEK-1 / JARA-ENERGY},
      ddc          = {530},
      cid          = {I:(DE-Juel1)IEK-1-20101013 / $I:(DE-82)080011_20140620$},
      pnm          = {1232 - Power-based Fuels and Chemicals (POF4-123)},
      pid          = {G:(DE-HGF)POF4-1232},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000700910700001},
      doi          = {10.1039/D1TA05240C},
      url          = {https://juser.fz-juelich.de/record/902340},
}