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| Hauptseite > Publikationsdatenbank > Data Collection Strategies, Analysis, and Interpretation in AP-XAS > print |
| Hauptseite > Publikationsdatenbank > Data Collection Strategies, Analysis, and Interpretation in AP-XAS > print |
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| 100 | 1 | _ | |a Müller, David |0 P:(DE-Juel1)166093 |b 0 |e Corresponding author |u fzj |
| 245 | _ | _ | |a Data Collection Strategies, Analysis, and Interpretation in AP-XAS |
| 260 | _ | _ | |a Washington, DC |c 2021 |b ACS Publications |
| 295 | 1 | 0 | |a Ambient Pressure Spectroscopy in Complex Chemical Environments |
| 300 | _ | _ | |a 315-331 |
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| 520 | _ | _ | |a This chapter will focus on strategies to collect meaningful X-ray absorption data in an ambient medium covering both the hard and soft X-ray regime and how to guide analysis, keeping experimental and physical differences of various strategies in mind. A special interest will be put on how the interaction of primary radiation and signal carriers with the surrounding medium will influence data acquisition and interpretation. Since hard and soft X-rays can be used to probe different electron shells in a material, both experiments can yield important and complementary information. Dipole selection rules lead to vastly different behavior of K- and L-edge XAS of transition metals, for example. In their ambient pressure variants, two major issues (that are fundamentally intertwined) arise when interpreting the data collected from both techniques: Whereas hard X-rays can penetrate condensed matter on a macroscopic scale making true transmission experiments possible, soft X-rays are confined to either electron or fluorescence yield detection modes, the latter suffering from low yields from lighter elements. Those not only pose different experimental challenges to avoid signal loss due to absorption in the reaction medium, but also probe depths of different orders of magnitude. |
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