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@ARTICLE{Cao:902642,
author = {Cao, Lei and Petracic, Oleg and Wei, Xian-Kui and Zhang,
Hengbo and Duchoň, Tomáš and Gunkel, Felix and
Koutsioumpas, Alexandros and Zhernenkov, Kirill and
Rushchanskii, Konstantin Z. and Hartmann, Heinrich and
Wilhelm, Marek and Li, Zichao and Xie, Yufang and He, Suqin
and Weber, Moritz L. and Veltruská, Kateřina and
Stellhorn, Annika and Mayer, Joachim and Zhou, Shengqiang
and Brückel, Thomas},
title = {{M}igration {K}inetics of {S}urface {I}ons in
{O}xygen‐{D}eficient {P}erovskite {D}uring {T}opotactic
{T}ransitions},
journal = {Small},
volume = {17},
number = {51},
issn = {1613-6810},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {FZJ-2021-04437},
pages = {2104356},
year = {2021},
abstract = {Oxygen diffusivity and surface exchange kinetics underpin
the ionic, electronic, and catalytic functionalities of
complex multivalent oxides. Towards understanding and
controlling the kinetics of oxygen transport in emerging
technologies, it is highly desirable to reveal the
underlying lattice dynamics and ionic activities related to
oxygen variation. In this study, the evolution of oxygen
content is identified in real-time during the progress of a
topotactic phase transition in La0.7Sr0.3MnO3-δ epitaxial
thin films, both at the surface and throughout the bulk.
Using polarized neutron reflectometry, a quantitative depth
profile of the oxygen content gradient is achieved, which,
alongside atomic-resolution scanning transmission electron
microscopy, uniquely reveals the formation of a novel
structural phase near the surface. Surface-sensitive X-ray
spectroscopies further confirm a significant change of the
electronic structure accompanying the transition. The
anisotropic features of this novel phase enable a distinct
oxygen diffusion pathway in contrast to conventional
observation of oxygen motion at moderate temperatures. The
results provide insights furthering the design of solid
oxygen ion conductors within the framework of topotactic
phase transitions.},
cin = {JCNS-2 / ER-C-2 / PGI-6 / PGI-7 / JCNS-FRM-II / PGI-1 /
ZEA-3 / PGI-4 / JARA-FIT},
ddc = {540},
cid = {I:(DE-Juel1)JCNS-2-20110106 / I:(DE-Juel1)ER-C-2-20170209 /
I:(DE-Juel1)PGI-6-20110106 / I:(DE-Juel1)PGI-7-20110106 /
I:(DE-Juel1)JCNS-FRM-II-20110218 /
I:(DE-Juel1)PGI-1-20110106 / I:(DE-Juel1)ZEA-3-20090406 /
I:(DE-Juel1)PGI-4-20110106 / $I:(DE-82)080009_20140620$},
pnm = {5233 - Memristive Materials and Devices (POF4-523) / 632 -
Materials – Quantum, Complex and Functional Materials
(POF4-632) / 6G4 - Jülich Centre for Neutron Research
(JCNS) (FZJ) (POF4-6G4)},
pid = {G:(DE-HGF)POF4-5233 / G:(DE-HGF)POF4-632 /
G:(DE-HGF)POF4-6G4},
experiment = {EXP:(DE-MLZ)MARIA-20140101},
typ = {PUB:(DE-HGF)16},
pubmed = {34791798},
UT = {WOS:000719613100001},
doi = {10.1002/smll.202104356},
url = {https://juser.fz-juelich.de/record/902642},
}