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@ARTICLE{Shams:902835,
author = {Shams, S. Fatemeh and Schmitz, Detlef and Smekhova,
Alevtina and Ghazanfari, Mohammad Reza and Giesen, Margret
and Weschke, Eugen and Chen, Kai and Luo, Chen and Radu,
Florin and Schmitz-Antoniak, Carolin},
title = {{E}lement-specific contributions to improved magnetic
heating of theranostic {C}o{F}e2{O}4 nanoparticles decorated
with {P}d},
journal = {Scientific reports},
volume = {11},
number = {1},
issn = {2045-2322},
address = {[London]},
publisher = {Macmillan Publishers Limited, part of Springer Nature},
reportid = {FZJ-2021-04592},
pages = {15843},
year = {2021},
abstract = {Decoration with Pd clusters increases the magnetic heating
ability of cobalt ferrite (CFO) nanoparticles by a factor of
two. The origin of this previous finding is unraveled by
element-specific X-ray absorption spectroscopy (XAS) and
magnetic circular dichroism (XMCD) combined with atomic
multiplet simulations and density functional theory (DFT)
calculations. While the comparison of XAS spectra with
atomic multiplet simulations show that the inversion degree
is not affected by Pd decoration and, thus, can be excluded
as a reason for the improved heating performance, XMCD
reveals two interrelated responsible sources: significantly
larger Fe and Co magnetic moments verify an increased total
magnetization which enhances the magnetic heating ability.
This is accompanied by a remarkable change in the
field-dependent magnetization particularly for Co ions which
exhibit an increased low-field susceptibility and a reduced
spin canting behavior in higher magnetic fields. Using DFT
calculations, these findings are explained by reduced
superexchange between ions on octahedral lattice sites via
oxygen in close vicinity of Pd, which reinforces the
dominating antiparallel superexchange interaction between
ions on octahedral and tetrahedral lattice sites and thus
reduces spin canting. The influence of the delocalized
nature of Pd 4d electrons on the neighboring ions is
discussed and the conclusions are illustrated with spin
density isosurfaces of the involved ions. The presented
results pave the way to design nanohybrids with tailored
electronic structure and magnetic properties.},
cin = {PGI-6},
ddc = {600},
cid = {I:(DE-Juel1)PGI-6-20110106},
pnm = {1212 - Materials and Interfaces (POF4-121)},
pid = {G:(DE-HGF)POF4-1212},
typ = {PUB:(DE-HGF)16},
pubmed = {34349172},
UT = {WOS:000684832300005},
doi = {10.1038/s41598-021-95189-y},
url = {https://juser.fz-juelich.de/record/902835},
}