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@ARTICLE{Lenz:902912,
author = {Lenz, Patrick and Hilgers, Fabienne and Burmeister, Alina
and Zimmermann, Leonie and Volkenborn, Kristina and
Grünberger, Alexander and Kohlheyer, Dietrich and Drepper,
Thomas and Jaeger, Karl-Erich and Knapp, Andreas},
title = {{T}he i{S}plit {GFP} assay detects intracellular
recombinant proteins in {B}acillus subtilis},
journal = {Microbial cell factories},
volume = {20},
number = {1},
issn = {1475-2859},
address = {London},
publisher = {Biomed Central},
reportid = {FZJ-2021-04667},
pages = {174},
year = {2021},
abstract = {BackgroundBacillus subtilis is one of the most important
microorganisms for recombinant protein production. It
possesses the GRAS (generally recognized as safe) status and
a potent protein secretion capacity. Secretory protein
production greatly facilitates downstream processing and
thus significantly reduces costs. However, not all
heterologous proteins are secreted and intracellular
production poses difficulties for quantification. To tackle
this problem, we have established a so-called intracellular
split GFP (iSplit GFP) assay in B. subtilis as a tool for
the in vivo protein detection during expression in batch
cultures and at a single-cell level. For the iSplit GFP
assay, the eleventh β-sheet of sfGFP is fused to a target
protein and can complement a detector protein consisting of
the respective truncated sfGFP (GFP1-10) to form fluorescent
holo-GFP.ResultsAs proof of concept, the GFP11-tag was fused
C-terminally to the E. coli β-glucuronidase GUS, resulting
in fusion protein GUS11. Variable GUS and GUS11 production
levels in B. subtilis were achieved by varying the ribosome
binding site via spacers of increasing lengths (4–12
nucleotides) for the GUS-encoding gene. Differences in
intracellular enzyme accumulation were determined by
measuring the GUS11 enzymatic activity and subsequently by
adding the detector protein to respective cell extracts.
Moreover, the detector protein was co-produced with the
GUS11 using a two-plasmid system, which enabled the in vivo
detection and online monitoring of glucuronidase production.
Using this system in combination with flow cytometry and
microfluidics, we were able to monitor protein production at
a single-cell level thus yielding information about
intracellular protein distribution and culture
heterogeneity.ConclusionOur results demonstrate that the
iSplit GFP assay is suitable for the detection,
quantification and online monitoring of recombinant protein
production in B. subtilis during cultivation as well as for
analyzing production heterogeneity and intracellular
localization at a single-cell level.},
cin = {IMET / IBG-1},
ddc = {570},
cid = {I:(DE-Juel1)IMET-20090612 / I:(DE-Juel1)IBG-1-20101118},
pnm = {2172 - Utilization of renewable carbon and energy sources
and engineering of ecosystem functions (POF4-217)},
pid = {G:(DE-HGF)POF4-2172},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:34488765},
UT = {WOS:000693256700003},
doi = {10.1186/s12934-021-01663-7},
url = {https://juser.fz-juelich.de/record/902912},
}