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@ARTICLE{Jelen:903586,
author = {Jelen, Andreja and Jang, Jae Hyuck and Oh, Junhyup and Kim,
Hae Jin and Meden, Anton and Vrtnik, Stane and Feuerbacher,
Michael and Dolinšek, Janez},
title = {{N}anostructure and local polymorphism in “ideal-like”
rare-earths-based high-entropy alloys},
journal = {Materials characterization},
volume = {172},
issn = {1044-5803},
address = {New York, NY},
publisher = {Science Direct},
reportid = {FZJ-2021-05240},
pages = {110837 -},
year = {2021},
abstract = {Rare-earths-based hexagonal high-entropy alloys (HEAs)
composed of the elements from the heavy half of the
lanthanide series (from Gd to Lu, with the exception of Yb)
and yttrium are much closer to an ideal solid solution than
HEAs composed of other elements from the entire periodic
system. Using the method of high-frequency levitation
melting, three candidates for a physical realization of an
ideal HEA were synthesized, an Y-Gd-Tb-Dy-Ho, a
Gd-Tb-Dy-Ho-Lu and a Tb-Dy-Ho-Er-Tm, and a study of their
structure and composition was performed to see how close to
ideal HEA samples can be prepared. We found that all three
HEAs exhibit a nanostructure of a hexagonal close-packed
(hcp) matrix and rod-like cubic close-packed (ccp)
precipitates of the lengths 200–600 nm and widths 50–100
nm. EDS analysis has revealed a general trend that the
precipitates are slightly enriched in the elements with
larger atomic radii relative to the matrix. The origin of
the nanostructure that represents a local hcp ↔ ccp
polymorphism at zero external pressure appear to be lattice
distortions (equivalent to a chemical pressure), occurring
due to the minute differences of the elements' atomic radii.
The volume per atom is slightly larger in the ccp
precipitates that are enriched in larger atoms, so that the
lattice distortions can be better accommodated and
minimized, which reduces the lattice strain energy that
contributes to the mixing enthalpy ΔHmix ≠ 0. The
employed synthesis route, which is standard for the
preparation of alloys of high structural quality, did not
lead to a physical realization of an ideal HEA in the most
promising theoretical candidates.},
cin = {ER-C-1},
ddc = {670},
cid = {I:(DE-Juel1)ER-C-1-20170209},
pnm = {5353 - Understanding the Structural and Functional Behavior
of Solid State Systems (POF4-535)},
pid = {G:(DE-HGF)POF4-5353},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000620963600006},
doi = {10.1016/j.matchar.2020.110837},
url = {https://juser.fz-juelich.de/record/903586},
}