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@ARTICLE{Sistla:904007,
author = {Sistla, Sree Koundinya and Mishra, Tarini Prasad and Deng,
Yuanbin and Kaletsch, Anke and Bram, Martin and Broeckmann,
Christoph},
title = {{P}olarity‐induced grain growth of gadolinium‐doped
ceria under field‐assisted sintering technology/spark
plasma sintering ({FAST}/{SPS}) conditions},
journal = {Journal of the American Ceramic Society},
volume = {104},
number = {5},
issn = {0002-7820},
address = {Westerville, Ohio},
publisher = {Soc.},
reportid = {FZJ-2021-05577},
pages = {1978 - 1996},
year = {2021},
abstract = {This study aims to understand the effect of the electrical
field on microstructure evolution during field-assisted
sintering or spark plasma sintering (FAST/SPS) of 10 $mol\%$
gadolinium-doped ceria (GDC) with experimental and numerical
methods. The novelty of this study has been the observation
of enhanced grain growth in the region closer to the anode,
even under FAST/SPS conditions with electrical fields less
than 5 V/cm. The grain growth kinetics, including
determination of activation energy and grain-boundary
mobility, were analyzed along the cross section of the
samples for different temperatures and dwell periods. With
an increase in distance from the anode, reduction in the
activation energy for grain growth and grain-boundary
mobility was observed. These observations attributed to the
attraction of oxygen ions to the anode region under an
electrical field with an increase in defects along the grain
boundaries. Thereby an increase in the grain-boundary
mobility and larger grains in that region were observed. A
homogenous microstructure was observed in a case where the
current did not flow through the sample. Furthermore, a
numerical strategy has also been developed to simulate this
behavior in addition to heat generation, heat transfer, and
densification using Finite Element Methods (FEM)
simulations. The simulation results provided an insight into
the presence of a potential difference across the cross
section of the samples. The simulation results were also in
good agreement with the experimental observations.},
cin = {IEK-1},
ddc = {660},
cid = {I:(DE-Juel1)IEK-1-20101013},
pnm = {1231 - Electrochemistry for Hydrogen (POF4-123)},
pid = {G:(DE-HGF)POF4-1231},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000608699300001},
doi = {10.1111/jace.17614},
url = {https://juser.fz-juelich.de/record/904007},
}