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@ARTICLE{Storion:904009,
author = {Storion, Ana G. and Lavagnini, Isabela R. and Campos, João
V. and da Silva, João G. P. and Maestrelli, Sylma C. and
Pallone, Eliria M. J. A.},
title = {{E}ffect of thermal insulation on microstructural
homogeneity and onset temperature of flash sintered
materials},
journal = {Journal of the European Ceramic Society},
volume = {41},
number = {15},
issn = {0955-2219},
address = {Amsterdam [u.a.]},
publisher = {Elsevier Science},
reportid = {FZJ-2021-05579},
pages = {7807 - 7815},
year = {2021},
abstract = {The present work aimed to reduce the microstructure
heterogeneity inherent to flash sintering by using alumina
blankets as a thermal insulator around ZnO cylindrical
samples during the sintering process, under different
electric field conditions. Thermal insulation significantly
reduced the flash onset temperature and the grain size
heterogeneity. For higher electric fields, a temperature
reduction as high as 480 °C was observed, which also led to
lower densification. These findings were discussed in terms
of changes in the heat loss dynamics coupled with the
adsorbed water retention, both promoted by the applied
thermal insulation. A model to estimate the temperature at
stage III of flash sintering was proposed. The final
temperature reached with thermal insulation did not differ
significantly from the ones without it. Thus, thermal
insulation could represent an alternative route to flash
sinter materials with lower furnace temperatures with energy
savings up to 78 $\%$ and a more homogeneous
microstructure.},
cin = {IEK-1},
ddc = {660},
cid = {I:(DE-Juel1)IEK-1-20101013},
pnm = {899 - ohne Topic (POF4-899)},
pid = {G:(DE-HGF)POF4-899},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000705091000007},
doi = {10.1016/j.jeurceramsoc.2021.08.060},
url = {https://juser.fz-juelich.de/record/904009},
}