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@ARTICLE{Xu:904014,
author = {Xu, Pengyu and Rheinheimer, Wolfgang and Mishra, Avanish
and Shuvo, Shoumya Nandy and Qi, Zhimin and Wang, Haiyan and
Dongare, Avinash M. and Stanciu, Lia A.},
title = {{O}rigin of {H}igh {I}nterfacial {R}esistance in
{S}olid‐{S}tate {B}atteries: {LLTO}/{LCO}
{H}alf‐{C}ells**},
journal = {ChemElectroChem},
volume = {8},
number = {10},
issn = {2196-0216},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {FZJ-2021-05584},
pages = {1847 - 1857},
year = {2021},
abstract = {The interface between cathode and electrolyte is a
significant source of large interfacial resistance in
solid-state batteries (SSBs). Spark plasma sintering (SPS)
allows densifying electrolyte and electrodes in one step,
which can improve the interfacial contact in SSBs and
significantly shorten the processing time. In this work, we
proposed a two-step joining process to prepare cathode
(LiCoO2, LCO)/electrolyte (Li0.33La0.57TiO3, LLTO) half
cells via SPS. Interdiffusion between Ti4+/Co3+ was observed
at the interface by SEM/STEM, resulting in the formation of
the Li−Ti−La−Co−O and Li−Ti−Co−O phases in
LLTO and the Li−Co−Ti−O phase in LCO. Computational
modeling was performed to verify that the Li−Ti−Co−O
phase has a LiTi2O4 host lattice. In a study of interfacial
electrical properties, the resistance of this interdiffusion
layer was found to be 105 Ω, which is 40 times higher
than the resistance of the individual LLTO phase. The
formation of an interdiffusion layer is identified as the
origin of the high interface resistance in the LLTO/LCO
half-cell.},
cin = {IEK-1},
ddc = {540},
cid = {I:(DE-Juel1)IEK-1-20101013},
pnm = {1221 - Fundamentals and Materials (POF4-122) / 1222 -
Components and Cells (POF4-122)},
pid = {G:(DE-HGF)POF4-1221 / G:(DE-HGF)POF4-1222},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000664255800014},
doi = {10.1002/celc.202100189},
url = {https://juser.fz-juelich.de/record/904014},
}