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@ARTICLE{Wang:904084,
author = {Wang, W. J. and Tan, X. Y. and Yang, S. P. and Luo, L. M.
and Zhu, X. Y. and Mao, Y. R. and Litnovsky, A. and Coenen,
J. W. and Linsmeier, Ch. and Wu, Yihui},
title = {{O}n grain growth and phase precipitation behaviors during
{W}-{C}r-{Z}r alloy densification using field-assisted
sintering technology},
journal = {International journal of refractory metals $\&$ hard
materials},
volume = {98},
issn = {0263-4368},
address = {Amsterdam [u.a.]},
publisher = {Elsevier Science},
reportid = {FZJ-2021-05654},
pages = {105552 -},
year = {2021},
note = {kein Zugriff auf Postprint},
abstract = {Field-assisted sintering technology (FAST), as a fast
densification method with low process temperature, was used
to manufacture self-passivating tungsten alloys (SPTAs) of
W-Cr-Zr in this work. To clarify the behaviors of grain
growth and Cr-rich phase precipitation under the action of
electric current during the densification process,
interrupted sintering at different temperatures (600–1000
°C) were performed. According to the viscous flow theory,
the activation energy of W-Cr-Zr sample for densification is
~23 kJ/mol. The differential form of power law was adopted
to evaluate the grain growth behavior. It is found that the
W-Cr-Zr alloy consolidated by FAST has a low activation
energy for grain growth of 82 kJ/mol. The Cr-rich phase
could be confirmed by XRD spectra even when the sintering
was interrupted at 600 °C. From the characterization of the
cross-sectional microstructure, the Cr-rich phases tend to
precipitate at sintering necks and defects (cracks/voids) in
particle interiors. The low formation temperature of the
Cr-rich phase is attributed to local overheating caused by
local high electric current. This work provides significant
insight into the mechanisms underlying the densification and
the evolution of the microstructure of the SPTAs during the
FAST process.},
cin = {IEK-4},
ddc = {670},
cid = {I:(DE-Juel1)IEK-4-20101013},
pnm = {1232 - Power-based Fuels and Chemicals (POF4-123)},
pid = {G:(DE-HGF)POF4-1232},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000663405100008},
doi = {10.1016/j.ijrmhm.2021.105552},
url = {https://juser.fz-juelich.de/record/904084},
}