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@ARTICLE{Wei:904343,
author = {Weiß, Lennart J. K. and Music, Emir and Rinklin, Philipp
and Straumann, Lea and Grob, Leroy and Mayer, Dirk and
Wolfrum, Bernhard},
title = {{E}ngineering {E}lectrostatic {R}epulsion of {M}etal
{N}anoparticles for {R}educed {A}dsorption in
{S}ingle-{I}mpact {E}lectrochemical {R}ecordings},
journal = {ACS applied nano materials},
volume = {4},
number = {8},
issn = {2574-0970},
address = {Washington, DC},
publisher = {ACS Publications},
reportid = {FZJ-2021-05913},
pages = {8314 - 8320},
year = {2021},
abstract = {Stochastic impact electrochemistry is a promising concept
to detect ultralow concentrations of nanoparticles in
solution. However, statistically reliable sensor outputs
require an appropriate number of observed nanoparticle
collision events. Here, arrays of individually addressable
electrodes allow increasing the effective detection area,
and thereby the number of collision events, without
sacrificing the signal-to-noise ratio. At the same time,
however, these measurements typically increase the
surface-to-volume ratio of the system, leading to a stronger
influence of adsorption on the number of available
particles. We address this issue of nanoparticle adsorption
by controlling the electrode–electrolyte interface close
to the detection electrodes. We use a direct nanoimpact
experiment to demonstrate that a negatively charged surface
leads to electrostatic repulsion, which results in a
2.5-fold increase in the number of detected collision
events. Adding to this improved sensor performance, a
tunable shield electrode offers a versatile tool to study
nanoparticle adsorption at the solid–liquid interface.},
cin = {IBI-3},
ddc = {540},
cid = {I:(DE-Juel1)IBI-3-20200312},
pnm = {5241 - Molecular Information Processing in Cellular Systems
(POF4-524)},
pid = {G:(DE-HGF)POF4-5241},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000692034900073},
doi = {10.1021/acsanm.1c01507},
url = {https://juser.fz-juelich.de/record/904343},
}