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000904589 1001_ $$0P:(DE-Juel1)145323$$aMoors, Marco$$b0
000904589 245__ $$aTiO x /Pt 3 Ti(111) surface-directed formation of electronically responsive supramolecular assemblies of tungsten oxide clusters
000904589 260__ $$aFrankfurt, M.$$bBeilstein-Institut zur Förderung der Chemischen Wissenschaften$$c2021
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000904589 520__ $$aHighly ordered titanium oxide films grown on a Pt3Ti(111) alloy surface were utilized for the controlled immobilization and tip-induced electric field-triggered electronic manipulation of nanoscopic W3O9 clusters. Depending on the operating conditions, two different stable oxide phases, z’-TiOx and w’-TiOx, were produced. These phases show a strong effect on the adsorption characteristics and reactivity of W3O9 clusters, which are formed as a result of thermal evaporation of WO3 powder on the complex TiOx/Pt3Ti(111) surfaces under ultra-high vacuum conditions. The physisorbed tritungsten nano-oxides were found as isolated single units located on the metallic attraction points or as supramolecular self-assemblies with a W3O9-capped hexagonal scaffold of W3O9 units. By applying scanning tunneling microscopy to the W3O9–(W3O9)6 structures, individual units underwent a tip-induced reduction to W3O8. At elevated temperatures, agglomeration and growth of large WO3 islands, which thickness is strongly limited to a maximum of two unit cells, were observed. The findings boost progress toward template-directed nucleation, growth, networking, and charge state manipulation of functional molecular nanostructures on surfaces using operando techniques.
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000904589 7001_ $$0P:(DE-HGF)0$$aAn, Yun$$b1
000904589 7001_ $$00000-0002-9458-4136$$aKuc, Agnieszka$$b2
000904589 7001_ $$0P:(DE-Juel1)167441$$aMonakhov, Kirill Yu$$b3$$eCorresponding author
000904589 773__ $$0PERI:(DE-600)2583584-1$$a10.3762/bjnano.12.16$$gVol. 12, p. 203 - 212$$p203 - 212$$tBeilstein journal of nanotechnology$$v12$$x2190-4286$$y2021
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