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@PHDTHESIS{Sietmann:906137,
author = {Sietmann, Michael},
title = {{P}otentialfeldmessungen zur {Q}ualitätsbewertung von
{B}ipolarplatten},
volume = {564},
school = {RWTH Aachen},
type = {Dissertation},
address = {Jülich},
publisher = {Forschungszentrum Jülich GmbH Zentralbibliothek, Verlag},
reportid = {FZJ-2022-01250},
isbn = {978-3-95806-606-9},
series = {Schriften des Forschungszentrums Jülich. Reihe Energie
$\&$ Umwelt / Energy $\&$ Environment},
pages = {ix, 160 S.},
year = {2021},
note = {RWTH Aachen, Diss., 2021},
abstract = {To make fuel cells accessible to a broader application,
cost reduction is necessary. An important component of the
fuel cell with great cost reduction potential is the bipolar
plate. At the same time, the quality of the bipolar plate is
of decisive importance for the function of a fuel cell and
its longevity. New test methods are needed for the quality
assurance of the bipolar plate. In this work, a method and a
test setup based on the propagation of the electric
potential field is developed for the detection of defects in
graphite composite bipolar plates and bipolar plate
materials. A current is passed through the bipolar plate via
a point contact. With measuring points around the contacting
point, the potential field in the bipolar plate can be
recorded and analyzed for disturbances. Central elements of
the test setup are two probes with 25 spring-loaded
measuring tips, which are moved over the bipolar plate.
Depending on the programming, the measuring tips conduct a
current through the sample or measure the potential field
forming in the sample. X-ray tomography and electrical
potential simulations are used as a reference and to
evaluate the measurement results of the test setup. The
measurement method is tested and potential measurement
uncertainties are identified on material strips of blank
plates with through holes as defined artificial defects. A
complex electrical conductivity network is formed in the
graphite composite bipolar plates by the graphite particles.
The conductivity network becomes visible as measurement
noise in the results of the potential field measurements.
The application of the measurement method to bipolar plates
is demonstrated on monopolar plates withone-sided flow
field, in which artificial defects are imitated by plastic
accumulations, admixed wood and steel particles. The plastic
accumulations represent non-conductive regions in the
bipolar plate and the wood particles represent isolated
defects such as cracks, voids or non-conductive foreign
bodies. Massive defects such as plastic accumulations can be
identified with the test setup and their local
manifestations determined. Isolated defects, on the other
hand, are not detected with the test setup. Ohmic resistance
measurements on the monopolar plates and cutouts from the
monopolar plates prove that only large-scale defects have a
negative influence on the electrical conductivity of bipolar
plates. Fuel cell tests with the monopolar plates confirm
the results of the ohmic resistance measurements, according
to which isolated defects have no influence on ohmic
resistance and fuel cell performance. The developed test
set-up is suitable for random measurement of electrical
properties and detection of performance-impairing defects in
bipolar plates.},
cin = {IEK-14},
cid = {I:(DE-Juel1)IEK-14-20191129},
pnm = {1231 - Electrochemistry for Hydrogen (POF4-123)},
pid = {G:(DE-HGF)POF4-1231},
typ = {PUB:(DE-HGF)3 / PUB:(DE-HGF)11},
urn = {urn:nbn:de:0001-2022040529},
url = {https://juser.fz-juelich.de/record/906137},
}