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@ARTICLE{Veelken:906583,
      author       = {Veelken, Philipp M. and Wirtz, Maike and Schierholz, Roland
                      and Tempel, Hermann and Kungl, Hans and Eichel, Rüdiger-A.
                      and Hausen, Florian},
      title        = {{I}nvestigating the {I}nterface between {C}eramic
                      {P}articles and {P}olymer {M}atrix in {H}ybrid
                      {E}lectrolytes by {E}lectrochemical {S}train {M}icroscopy},
      journal      = {Nanomaterials},
      volume       = {12},
      number       = {4},
      issn         = {2079-4991},
      address      = {Basel},
      publisher    = {MDPI},
      reportid     = {FZJ-2022-01534},
      pages        = {654 -},
      year         = {2022},
      abstract     = {The interface between ceramic particles and a polymer
                      matrix in a hybrid electrolyte is studied with high spatial
                      resolution by means of Electrochemical Strain Microscopy
                      (ESM), an Atomic Force Microscope (AFM)-based technique. The
                      electrolyte consists of polyethylene oxide with lithium
                      bis(trifluoromethanesulfonyl)imide (PEO6–LiTFSI) and
                      Li6.5La3Zr1.5Ta0.5O12 (LLZO:Ta). The individual components
                      are differentiated by their respective contact resonance,
                      ESM amplitude and friction signals. The ESM signal shows
                      increased amplitudes and higher contact resonance
                      frequencies on the ceramic particles, while lower amplitudes
                      and lower contact resonance frequencies are present on the
                      bulk polymer phase. The amplitude distribution of the hybrid
                      electrolyte shows a broader distribution in comparison to
                      pure PEO6–LiTFSI. In the direct vicinity of the particles,
                      an interfacial area with enhanced amplitude signals is
                      found. These results are an important contribution to
                      elucidate the influence of the ceramic–polymer interaction
                      on the conductivity of hybrid electrolytes.},
      cin          = {IEK-9},
      ddc          = {540},
      cid          = {I:(DE-Juel1)IEK-9-20110218},
      pnm          = {HITEC - Helmholtz Interdisciplinary Doctoral Training in
                      Energy and Climate Research (HITEC) (HITEC-20170406) / 1223
                      - Batteries in Application (POF4-122)},
      pid          = {G:(DE-Juel1)HITEC-20170406 / G:(DE-HGF)POF4-1223},
      typ          = {PUB:(DE-HGF)16},
      pubmed       = {35214982},
      UT           = {WOS:000812558300001},
      doi          = {10.3390/nano12040654},
      url          = {https://juser.fz-juelich.de/record/906583},
}