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@ARTICLE{Schfer:906838,
author = {Schäfer, Dominik and Queda, Larissa and Nischwitz, Volker
and Fang, Qingping and Blum, Ludger},
title = {{O}rigin of {S}team {C}ontaminants and {D}egradation of
{S}olid-{O}xide {E}lectrolysis {S}tacks},
journal = {Processes},
volume = {10},
number = {3},
issn = {2227-9717},
address = {Basel},
publisher = {MDPI},
reportid = {FZJ-2022-01732},
pages = {598},
year = {2022},
abstract = {Two once-through steam generators and a combination of a
steam generator and a gas preheater for supplying feed gases
to solid-oxide electrolysis stacks were evaluated for their
carryover characteristics of contaminants from the
feed-water into the steam phase. The concentrations of
various trace impurities in the steam were determined by
sampling the steam condensates and screening them with
inductively coupled plasma–mass spectrometry for 19
elements and liquid ion chromatography and continuous flow
analysis for chloride and ammonium. Steam-soluble species
such as boric acid undergo complete volatilization and
transfer into the steam phase. During unstable evaporation
in the steam generators an extensive physical carryover of
alloying metal species was observed. At realistic operation
conditions for steam electrolysis, the gas preheater caused
a considerable release of silicon into the steam phase. Two
stack experiments were performed with common preheater
temperatures and showed largely increased cell voltage
degradation at higher operation temperatures. The post-test
chemical analysis of cell samples revealed significant
concentrations of silicon in the samples that are regarded
as primary cause for increased degradation. These findings
could partially explain the wide spread of degradation rates
reported for solid-oxide steam electrolysis experiments.},
cin = {IEK-9 / ZEA-3 / IEK-14},
ddc = {570},
cid = {I:(DE-Juel1)IEK-9-20110218 / I:(DE-Juel1)ZEA-3-20090406 /
I:(DE-Juel1)IEK-14-20191129},
pnm = {1231 - Electrochemistry for Hydrogen (POF4-123) / 1232 -
Power-based Fuels and Chemicals (POF4-123) / Verbundvorhaben
P2X-2: Erforschung, Validierung und Implementierung von
'Power-to-X' Konzepten ' Teilvorhaben Z0-2 (03SFK2Z0-2)},
pid = {G:(DE-HGF)POF4-1231 / G:(DE-HGF)POF4-1232 /
G:(BMBF)03SFK2Z0-2},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000774438700001},
doi = {10.3390/pr10030598},
url = {https://juser.fz-juelich.de/record/906838},
}