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@ARTICLE{Heidrich:906960,
author = {Heidrich, Bastian and Pritzlaff, Lars and Börner, Markus
and Winter, Martin and Niehoff, Philip},
title = {{C}omparative {X}-ray {P}hotoelectron {S}pectroscopy
{S}tudy of the {SEI} and {CEI} in {T}hree {D}ifferent
{L}ithium {I}on {C}ell {F}ormats},
journal = {Journal of the Electrochemical Society},
volume = {169},
number = {3},
issn = {0013-4651},
address = {Bristol},
publisher = {IOP Publishing},
reportid = {FZJ-2022-01778},
pages = {030533 -},
year = {2022},
abstract = {The solid electrolyte interphase (SEI) and cathode
electrolyte interphase (CEI) of three lithium ion cell
formats, i.e., coin, lab-scale pouch and multi-layer pouch,
are compared. Half the cells are additionally dried prior to
electrolyte filling and cycling. The highest water content
per cell, determined by Karl Fischer titration, is found for
lab-scale pouch cells due to their disadvantageous ratio of
cell housing area to electrode area. The water content
influences the performance during electrochemical formation
as well as the impedance. This is linked to increasing
lithium fluoride concentration, as determined by X-ray
photoelectron spectroscopy. For dried cells, this is not the
case because there is less conducting salt hydrolysis. The
CEI thickness decreases for dried pouch cells, while the
organic SEI thickness increases in all cell formats for
dried cells. It is concluded that the initial thickness of
the porous organic SEI depends on the insulation of the
dense inorganic SEI close to the electrode surface. Organic
species are more likely to contribute to negative electrode
passivation when the extent of conducting salt hydrolysis is
low. For coin cells, the presence of atmospheric gases
during formation results in thicker SEI and CEI, no matter
whether cells are additionally dried.},
cin = {IEK-12},
ddc = {660},
cid = {I:(DE-Juel1)IEK-12-20141217},
pnm = {1221 - Fundamentals and Materials (POF4-122)},
pid = {G:(DE-HGF)POF4-1221},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000770136300001},
doi = {10.1149/1945-7111/ac5c08},
url = {https://juser.fz-juelich.de/record/906960},
}