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@ARTICLE{Atik:906974,
author = {Atik, Jaschar and Winter, Martin and Paillard, Elie},
title = {{L}ocal superconcentration via solvating ionic liquid
electrolytes for safe 4.3{V} lithium metal batteries},
journal = {Electrochimica acta},
volume = {415},
issn = {0013-4686},
address = {New York, NY [u.a.]},
publisher = {Elsevier},
reportid = {FZJ-2022-01787},
pages = {140181 -},
year = {2022},
abstract = {A novel solvating ionic liquid (SIL), N-methyl
N-oligo(ethylene oxide)pyrrolidinium
bis(fluorosulfonyl)imide (Pyr1,(2O)7FSI) was synthesized and
used to prepare binary and ternary liquid electrolytes with
LiFSI as conducting salt and
1,1,2,2-tetrafluoroethyl-2,2,2-trifluoroethyl ether (TTE) as
a non-solvating low viscosity co-solvent. Thereby, the
binary superconcentrated liquid electrolyte (i.e., 6.8 m
LiFSI in Pyr1,(2O)7FSI) reaches a Li+ ion transference
number of 0.25 ± 0.02. To enhance the ionic conductivity
and separator wetting, the binary electrolyte was mixed with
TTE leading to local superconcentrated Li+ ion solvation
structures as shown by Raman measurements. These ternary
electrolytes exhibit improved wettability, excellent safety
and allow cycling in NMC622||Li cells and Cu||Li cells with
Coulombic efficiencies of up to $99.9\%$ and $98.5\%,$
respectively, and a capacity retention of $84\%$ for
NMC622||Li cells with the electrolyte 2.0 m LiFSI,
Pyr1,(2O)7FSI:TTE (1:1 $wt\%)$ after 100 cycles vs. a cell
failure after 35 cycles for the state-of-the-art containing
IL N‑butyl‑N-methylpyrrolidinium FSI electrolyte.},
cin = {IEK-12},
ddc = {540},
cid = {I:(DE-Juel1)IEK-12-20141217},
pnm = {1221 - Fundamentals and Materials (POF4-122)},
pid = {G:(DE-HGF)POF4-1221},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000872022700001},
doi = {10.1016/j.electacta.2022.140181},
url = {https://juser.fz-juelich.de/record/906974},
}