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@ARTICLE{Hou:907595,
author = {Hou, Hui and Mariani, Alessandro and Suo, Yanpeng and Gao,
Xinpei and Giffin, Jürgen and Rodenbücher, Christian and
Passerini, Stefano and Korte, Carsten},
title = {{T}uning {P}olybenzimidazole {M}embrane by {I}mmobilizing a
{N}ovel {I}onic {L}iquid with {S}uperior {O}xygen
{R}eduction {R}eaction {K}inetics},
journal = {Chemistry of materials},
volume = {34},
number = {10},
issn = {0897-4756},
address = {Washington, DC},
publisher = {American Chemical Society},
reportid = {FZJ-2022-02099},
pages = {acs.chemmater.1c03819},
year = {2022},
abstract = {Protic ionic liquid (PIL) is a promising nonaqueous
electrolyte alternative to replacing phosphoric acid for
fuel cells operating at temperatures above 100 °C. In this
study, the physical and electrochemical properties of
stoichiometric and nonstoichiometric PILs are investigated
focusing on their acid/base ratio. The study involves a
series of PILs, generically indicated as
N,N-diethyl-3-sulfopropane-1-ammonium
trifluoromethanesulfonate ([DESPA+][TfO–]), varying from
an excess of the proton acceptor
(N,N-diethyl-3-aminopropane-1-sulfonic acid) to an excess of
the proton donor (trifluoromethanesulfonic acid, TfOH).
Compared to a state-of-the-art electrolyte, i.e.,
concentrated phosphoric acid, the nonstoichiometric
[DESPA+][TfO–] shows superior oxygen reduction reaction
kinetics on the investigated Pt catalysts and oxygen
permeation ability (DO2·cO2). [DESPA+][TfO–] with a
base-to-acid molar ratio of 1:2 achieves a current density
∼10 times larger than that of concentrated phosphoric acid
at 110 °C and 0.8 V. Membranes including polybenzimidazole
as a host polymer and stoichiometric and nonstoichiometric
[DESPA+][TfO–] as the conductive electrolyte exhibit
promising properties in terms of thermal stability and
conductivity. At 120 °C and $40\%$ relative humidity,
conductivities of 2 and 16 mS cm–1 are achieved by the
membranes employing stoichiometric and excess acid
[DESPA+][TfO–], respectively.},
cin = {IEK-14},
ddc = {540},
cid = {I:(DE-Juel1)IEK-14-20191129},
pnm = {1231 - Electrochemistry for Hydrogen (POF4-123)},
pid = {G:(DE-HGF)POF4-1231},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000805874800005},
doi = {10.1021/acs.chemmater.1c03819},
url = {https://juser.fz-juelich.de/record/907595},
}