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@ARTICLE{Wetzel:907710,
      author       = {Wetzel, Oliver and Prymak, Oleg and Loza, Kateryna and
                      Gumbiowski, Nina and Heggen, Marc and Bayer, Peter and
                      Beuck, Christine and Weidenthaler, Claudia and Epple,
                      Matthias},
      title        = {{W}ater-{B}ased {S}ynthesis of {U}ltrasmall {N}anoparticles
                      of {P}latinum {G}roup {M}etal {O}xides (1.8 nm)},
      journal      = {Inorganic chemistry},
      volume       = {61},
      number       = {12},
      issn         = {0020-1669},
      address      = {Washington, DC},
      publisher    = {American Chemical Society},
      reportid     = {FZJ-2022-02173},
      pages        = {5133 - 5147},
      year         = {2022},
      abstract     = {Ultrasmall nanoparticles of platinum group metal oxides
                      (core diameter of about 1.8 nm) were prepared by alkaline
                      hydrolysis of metal precursors in the presence of NaBH4 and
                      by colloidal stabilization with tripeptide glutathione. We
                      obtained water-dispersed nanoparticles of Rh2O3, PdO, RuO2,
                      IrO2, Os/OsO2, and Pt/PtO. Their size was probed using
                      high-resolution transmission electron microscopy,
                      differential centrifugal sedimentation, small-angle X-ray
                      scattering, and diffusion-ordered 1H NMR spectroscopy (1H
                      DOSY). Their oxidation state was clearly determined using
                      X-ray photoelectron spectroscopy, X-ray powder diffraction,
                      and electron diffraction. The chemical composition of the
                      nanoparticles, that is, the ratio of the metal oxide core
                      and glutathione capping agent, was quantitatively determined
                      by a combination of these methods.},
      cin          = {ER-C-1},
      ddc          = {540},
      cid          = {I:(DE-Juel1)ER-C-1-20170209},
      pnm          = {5351 - Platform for Correlative, In Situ and Operando
                      Characterization (POF4-535)},
      pid          = {G:(DE-HGF)POF4-5351},
      typ          = {PUB:(DE-HGF)16},
      pubmed       = {35285631},
      UT           = {WOS:000779822100034},
      doi          = {10.1021/acs.inorgchem.2c00281},
      url          = {https://juser.fz-juelich.de/record/907710},
}