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000907713 1001_ $$00000-0001-5823-3665$$aGuasco, L.$$b0
000907713 245__ $$aResonant neutron reflectometry for hydrogen detection
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000907713 520__ $$aThe detection and quantification of hydrogen is becoming increasingly important in research on electronic materials and devices, following the identification of the hydrogen content as a potent control parameter for the electronic properties. However, establishing quantitative correlations between the hydrogen content and the physical properties of solids remains a formidable challenge. Here we report neutron reflectometry experiments on 50 nm thick niobium films during hydrogen loading, and show that the momentum-space position of a prominent waveguide resonance allows tracking of the absolute hydrogen content with an accuracy of about one atomic percent on a timescale of less than a minute. Resonance-enhanced neutron reflectometry thus allows fast, direct, and non-destructive measurements of the hydrogen concentration in thin-film structures, with sensitivity high enough for real-time in-situ studies.
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000907713 7001_ $$00000-0001-9945-8342$$aKhaydukov, Yu. N.$$b1
000907713 7001_ $$0P:(DE-Juel1)142052$$aPütter, S.$$b2
000907713 7001_ $$00000-0001-7307-1545$$aSilvi, L.$$b3
000907713 7001_ $$00000-0002-3479-2830$$aPaulin, M. A.$$b4
000907713 7001_ $$0P:(DE-HGF)0$$aKeller, T.$$b5
000907713 7001_ $$00000-0001-5220-9023$$aKeimer, B.$$b6$$eCorresponding author
000907713 773__ $$0PERI:(DE-600)2553671-0$$a10.1038/s41467-022-29092-z$$gVol. 13, no. 1, p. 1486$$n1$$p1486$$tNature Communications$$v13$$x2041-1723$$y2022
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