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| Hauptseite > Publikationsdatenbank > The in situ generated emerging phase inside dual phase oxygen transport membranes > print |
| Hauptseite > Publikationsdatenbank > The in situ generated emerging phase inside dual phase oxygen transport membranes > print |
| 001 | 907873 | ||
| 005 | 20240709082153.0 | ||
| 024 | 7 | _ | |a 10.1016/j.actamat.2022.118034 |2 doi |
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| 100 | 1 | _ | |a Ran, Ke |0 P:(DE-Juel1)174238 |b 0 |e Corresponding author |u fzj |
| 245 | _ | _ | |a The in situ generated emerging phase inside dual phase oxygen transport membranes |
| 260 | _ | _ | |a Amsterdam [u.a.] |c 2022 |b Elsevier Science |
| 336 | 7 | _ | |a article |2 DRIVER |
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| 520 | _ | _ | |a The in situ generated emerging phase inside the dual-phase oxygen transport membranes (DP-OTMs) plays a crucial role in boosting the overall performance of DP-OTMs. However, its detailed structure and properties are still not fully understood. Utilizing advanced transmission electron microscopy (TEM) techniques, the emerging phase GdxCe1-xFeyCo1-yO3-δ (GCFCO) inside the CexGd1-xO2-δ-FeCo2O4 (CGO-FC2O) OTMs was successfully characterized at the atomic scale. The newly formed GCFCO is primarily surrounded by the CGO, and contributes to a significant reduction of non-solute segregation at the CGO grain boundaries. Electronic characteristics of the GCFCO shows a sensitive dependence on its chemical composition, including the valence state of Ce and Fe as well as the oxygen vacancies. Additional CGO-GCFCO interfaces were introduced, where almost intact crystal structures were observed with slight Gd and Co segregation ∼1 nm at the edges. Approaching the interface, on the CGO side, only a minimum drop of the Ce valence was determined. On the GCFCO side, mixed Ce3+ and Ce4+ are partially occupying the Gd sites, while Fe and Co valence stay constant until the edge. Our study provides novel insight into the phase information within CGO-FC2O composites, which paves the path towards superior performance of various DP-OTMs |
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| 536 | _ | _ | |a DFG project 387282673 - Die Rolle von Grenzflächen in mehrphasigen Ceroxid-basierten Membranen für den Einsatz in Membranreaktoren |0 G:(GEPRIS)387282673 |c 387282673 |x 1 |
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| 773 | _ | _ | |a 10.1016/j.actamat.2022.118034 |g Vol. 234, p. 118034 - |0 PERI:(DE-600)2014621-8 |p 118034 |t Acta materialia |v 234 |y 2022 |x 1359-6454 |
| 856 | 4 | _ | |u https://juser.fz-juelich.de/record/907873/files/emerging%2Bphase%2Binside%2BOTM.pdf |y Published on 2022-05-19. Available in OpenAccess from 2024-05-19. |
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