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@PHDTHESIS{Bischof:908235,
author = {Bischof, Oliver},
title = {{A}pplication-{S}pecific {C}alibration of {C}ondensation
{P}article {C}ounters under {L}ow {P}ressure {C}onditions},
volume = {579},
school = {RWTH Aachen University},
type = {Dissertation},
address = {Jülich},
publisher = {Forschungszentrum Jülich GmbH Zentralbibliothek, Verlag},
reportid = {FZJ-2022-02478},
isbn = {978-3-95806-629-8},
series = {Schriften des Forschungszentrums Jülich Reihe Energie $\&$
Umwelt / Energy $\&$ Environment},
pages = {ix, 137},
year = {2022},
note = {Dissertation, RWTH Aachen University, 2021},
abstract = {Condensation Particle Counters (CPC) are research
instruments that are commonly used to measure fine, airborne
particles. They are able to determine the particle number
concentration of both, the smallest nanoparticles and also
larger particles in the accumulation mode, which cannot be
measured with optical methods at all or with sufficient
accuracy. In the last four decades, CPCs have been
increasingly used todetermine particle number concentrations
also at non-standard atmospheric pressurein both scientific
research as well as for regulatory purposes. Measurement
conditionsat reduced pressure require a dedicated
calibration of the CPCs to ensure correctresults. The aim of
my thesis was to investigate the performance of CPCs at
variouslevels of low-pressure by means of a comprehensive
and detailed calibration study.In the first part, this
thesis reviews details of the CPC technology, explains
applicationswith a need for low-pressure calibration and
presents an extensive literature review ofthe field. It
provides a critical analysis of the papers most relevant to
this research,building on a survey of more than 60
peer-reviewed publications from the past forty years. The
literature review points to contradictions in the
understanding of thebehavior of CPCs at low pressure and
highlights opposing findings. In a subsequentsection, a
numerical model is applied to investigate how reduced
pressure conditionsimpact CPC performance in theory. The
model delivers a prediction of CPC countingefficiencies as
well as d90, d50 and d10 cut-sizes at various levels of
reduced pressure.The second part of this thesis describes
extensive laboratory experiments and providesa detailed
analysis of the performance at reduced pressure. Two
different CPC modelswere calibrated for their particle
counting efficiency, smallest particle size detectionlimit,
and concentration linearity. The calibrations were performed
with test aerosols oftwo very different particle sources.
One of the calibration aerosols is representative
ofinorganic particles in ambient air not impacted by
anthropogenic activity. The otheraerosol is freshly
generated soot from an inverted-flame burner, which serves
as aproxy for combustion emissions found in urban
environments. Additionally, all countingefficiency
experiments were done with the relative humidity of the
calibration aerosolvaried from almost dry to moderate levels
of humidity. This aspect was included toconsider that
humidity might play a role in the activation of particles
inside a CPC.This thesis provides new insights into the
experimental method, operating parametersand effective
practices to calibrate CPCs for their use under low-pressure
conditions.Results demonstrate that in general CPCs work as
specified down to a thresholdpressure. Below that point,
their performance depends on the exact measurementconditions
and the specific CPC design. These findings are an important
advancementin understanding the behavior of CPCs at low
pressure and can serve as guidancewhen correcting the
reported number concentration for the impact of reduced
pressure.They also show that a dedicated calibration of CPCs
is advisable for every type of lowpressureapplication that
requires highly accurate particle number concentration
data.},
cin = {IEK-8},
cid = {I:(DE-Juel1)IEK-8-20101013},
pnm = {899 - ohne Topic (POF4-899)},
pid = {G:(DE-HGF)POF4-899},
typ = {PUB:(DE-HGF)3 / PUB:(DE-HGF)11},
url = {https://juser.fz-juelich.de/record/908235},
}