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@INPROCEEDINGS{Ivanova:908323,
author = {Ivanova, Mariya and Schäfer, Laura-Alena and Zeng, Yuan
and Deibert, Wendelin and Menzler, Norbert H. and Guillon,
Olivier},
title = {{E}ffect of sintering conditions on the phase and
microstructure features of
{B}a1.015{Z}r0.8-x{C}e0.2{Y}x{O}3-δ proton conducting cell
components},
reportid = {FZJ-2022-02542},
year = {2022},
abstract = {Ceramic proton conductors of the type
Ba1.015Zr0.8-xCe0.2YxO3-δ (BZCY) where x = 0.175 and 0.24
were prepared via a modified reactive solid state synthesis
route from stoichiometric mixtures of BaCO3 and the
corresponding oxides under addition of minor amount of NiO
as a sintering aid. Ba excess of 1.5 mol. $\%$ was added to
compensate possible Ba evaporation during the thermal
treatments as reported previously. From the pre-heated
powders half-cell assemblies consisting of a BZCY solid
electrolyte layer on BZCY:NiO anode support were prepared
via tape casting and compared after sintering at various
conditions to reference pellets with equivalent compositions
and prepared under similar conditions. The aim was to
correlate the phase and microstructure features of the BZCY
electrolyte layer to the presence of a supporting NiO rich
layer and thus providing optimal parameters for sintering of
such bi-layers with homogeneous phase composition, i.e.
minimization of the secondary phase shares, and finally,
proving the hypothesis that the BZCY:NiO anode composite is
potentially much stronger sink for BaO than the gas phase.},
month = {Jun},
date = {2022-06-07},
organization = {6th International Workshop Prospects
on Proton Ceramic Cells, Dijon
(France), 7 Jun 2022 - 10 Jun 2022},
subtyp = {After Call},
cin = {IEK-1},
cid = {I:(DE-Juel1)IEK-1-20101013},
pnm = {1231 - Electrochemistry for Hydrogen (POF4-123) / SOFC -
Solid Oxide Fuel Cell (SOFC-20140602)},
pid = {G:(DE-HGF)POF4-1231 / G:(DE-Juel1)SOFC-20140602},
typ = {PUB:(DE-HGF)6},
url = {https://juser.fz-juelich.de/record/908323},
}