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@ARTICLE{Chen:908769,
author = {Chen, Yingzhen and Endres, Manuel B. and Giffin, Jürgen
and Korte, Carsten},
title = {{I}nvestigation of the protolytic equilibrium of a highly
{B}rønsted acidic ionic liquid and residual water using
{R}aman spectroscopy},
journal = {Journal of molecular liquids},
volume = {345},
issn = {0167-7322},
address = {New York, NY [u.a.]},
publisher = {Elsevier},
reportid = {FZJ-2022-02825},
pages = {117796 -},
year = {2022},
abstract = {Protic ionic liquids (PILs) are promising candidates as
non-aqueous proton-conducting electrolytes for use in
polymer electrolyte membrane fuel cells with operating
temperatures over 100 °C. 2-sulfoethylammonium triflate
[2-Sea][TfO] is one such PIL electrolyte, in which the
highly Brønsted acidic sulfoalkylammonium cations act as
mobile protonic charge carriers and proton donors. In order
to gain a molecular-level understanding of proton transfer
in a PIL electrolyte containing a small amount of residual
water from fuel cell operation, the protolytic equilibrium
of the highly acidic cation was investigated by means of
Raman spectroscopy. Density functional theory (DFT)
calculations were conducted to identify the vibration modes
sensitive to protonation and to gain information on the
possible conformation of the cation. The deprotonation of
the 2-sulfoethylammonium cation resulted in a characteristic
upward frequency shift in the ν(SC) stretching vibration.
An equilibrium constant of 0.23 ± 0.09 was calculated for
the protolytic reaction, indicating [2-Sea][TfO] as a
promising proton donor for the fuel cell application.},
cin = {IEK-14},
ddc = {540},
cid = {I:(DE-Juel1)IEK-14-20191129},
pnm = {1231 - Electrochemistry for Hydrogen (POF4-123)},
pid = {G:(DE-HGF)POF4-1231},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000713883900016},
doi = {10.1016/j.molliq.2021.117796},
url = {https://juser.fz-juelich.de/record/908769},
}