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@INPROCEEDINGS{Klinkenberg:909871,
author = {Klinkenberg, Martina and Marques Fernandes, M. and Baeyens,
B. and Bosbach, D. and Brandt, F.},
title = {{R}etention of 226{R}a by montmorillonite},
reportid = {FZJ-2022-03480},
year = {2022},
abstract = {Although 226Ra is a critical radionuclide in the safety
analysis for deep geological disposal of spent nuclear fuel,
adsorption data for 226Ra onto clay minerals are sparse in
the open literature. So far, the adsorption and diffusion of
226Ra in clay minerals is assumed similar to that for Sr and
Ba, based on chemical analogy. In this study, we present new
experimental data that improves the quantitative
understanding of the retention of 226Ra in 2:1 clay minerals
relevant for radioactive waste disposal. Montmorillonite as
a major constituent of bentonite (up to 90 $wt.-\%)$ is an
important sink for potentially released radionuclides. To
study the 226Ra adsorption behaviour on bentonites,
adsorption experiments were carried out onto the homo-ionic
Na form of Wyoming montmorillonite (SWy-2) in diluted
systems and compared to the adsorption of Ba under the same
conditions. 226Ra and Ba adsorption edges in the pH range 5
to 10 at different ionic strengths (0.01 - 0.3 M NaCl) and
an isotherm (pH 7, 10-9 M < [Ra,Ba] > 10-2 M) were carried
out on Na-SWy. Our results c The 2-site Protolysis Non
Electrostatic Surface Complexation and Cation Exchange
adsorption model reproduces the experimental data for both
elements quite well. The Kc values for Ba2+-Na+ and
226Ra2+-Na+ exchange equilibria are in good agreement at low
ionic strength (log Kc = 0.70 - 0.84), whereas at high ionic
strength, the Kc (Ba-Na) is slightly higher (log Kc of 0.90
(0.3 M) vs 0.70 (≤ 0.02 M)). In contrast, the Kc (Ra-Na)
exhibits a clear dependency on ionic strength, with log Kc
values of 0.7, 1.14 and 1.34 at NaCl background
concentrations of 0.01/0.02 M, 0.14 M and 0.3 M,
respectively. The results presented here indicate that Ba
can be used as a good analogue for 226Ra regarding the
adsorption on montmorillonite at ionic strengths < 0.1 M and
pH < 8, but deviates in its behaviour at higher ionic
strength. This evident higher selectivity of Ra on Na-SWy
may be due to the larger ionic radius of Ra compared to Ba.
The contribution of surface complexation to the overall
adsorption is the same for Ba and Ra and is independent of
ionic strength.},
month = {Jun},
date = {2022-06-13},
organization = {8th International Conference on Clays
in Natural and Engineered Barriers for
Radioactive Waste Confinement, Nancy
(France), 13 Jun 2022 - 16 Jun 2022},
subtyp = {Other},
cin = {IEK-6},
cid = {I:(DE-Juel1)IEK-6-20101013},
pnm = {1411 - Nuclear Waste Disposal (POF4-141) / EURAD - European
Joint Programme on Radioactive Waste Management (847593)},
pid = {G:(DE-HGF)POF4-1411 / G:(EU-Grant)847593},
typ = {PUB:(DE-HGF)24},
url = {https://juser.fz-juelich.de/record/909871},
}