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@INPROCEEDINGS{Basak:912070,
author = {Basak, Shibabrata and Park, Junbeom and Eichel,
Rüdiger-A.},
title = {{V}isualization of active solid-gas interface using in situ
{TEM}},
reportid = {FZJ-2022-05297},
year = {2022},
abstract = {Power-to-X enables the production of valuable compounds
from the CO2 via catalytic reaction for net-zero carbon
economy. The understanding of the behaviors of the supported
catalyst under the reaction conditions and the elucidating
the associated mechanism are crucial for the rational design
of high-performing catalyst materials. The understanding and
atomic level information provided by aberration-corrected
TEM is unparalleled, particularly for the study of catalyst
nanoparticles. Post-mortem analysis can make it difficult to
underpin the specifics of a catalytic reaction mechanism,
without being able to observe the structures under a
realistic environment. The development of specialized
microelectromechanical systems (MEMS) based sample holder
now allows us to contain gas near the sample at more than 1
bar pressure with precise control over heat, gas flow and
gas compositions},
month = {Aug},
date = {2022-08-31},
organization = {3rd ELECTRA Symposium, RWTH Aachen
(Germany), 31 Aug 2022 - 1 Sep 2022},
subtyp = {After Call},
cin = {IEK-9 / ER-C},
cid = {I:(DE-Juel1)IEK-9-20110218 / I:(DE-Juel1)ER-C-20211020},
pnm = {1232 - Power-based Fuels and Chemicals (POF4-123) / iNEW2.0
(BMBF-03SF0627A) / Electroscopy - Electrochemistry of
All-solid-state-battery Processes using Operando Electron
Microscopy (892916)},
pid = {G:(DE-HGF)POF4-1232 / G:(DE-Juel1)BMBF-03SF0627A /
G:(EU-Grant)892916},
typ = {PUB:(DE-HGF)24},
url = {https://juser.fz-juelich.de/record/912070},
}