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000941216 1001_ $$0P:(DE-HGF)0$$aFaassen, Fabian$$b0
000941216 245__ $$aBifunctionalized Polyoxotungstates: Dilacunary Keggin Clusters Incorporating Fe III and Organoarsonate Constituents
000941216 260__ $$aWashington, DC$$bACS Publ.$$c2023
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000941216 520__ $$aPolyanions [{B-α-(OH)Fe2(PW10O37)}2{o-R–C6H4–AsO3)}2]12– (R = NH2 (1) and NO2 (2)) represent the first polyoxotungstates functionalized by both organoarsonates and FeIII. 1 and 2 comprise the rare dilacunary Keggin-type phosphotungstate {B-α-PW10O37}9– isomer that coordinates FeIII ions to form {B-α-FeIII2PW10} complexes linked into dimers via two organoarsonate groups. The title polyanions have been isolated as crystalline materials and fully characterized via single-crystal and powder X-ray diffraction, elemental analysis and IR and UV–vis spectroscopies, including solution stability studies. In addition, their electrochemical and magnetic properties have been characterized.
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000941216 7001_ $$0P:(DE-Juel1)157892$$aIzarova, Natalya V.$$b1
000941216 7001_ $$00000-0003-3688-631X$$avan Leusen, Jan$$b2
000941216 7001_ $$0P:(DE-Juel1)130782$$aKögerler, Paul$$b3$$eCorresponding author
000941216 773__ $$0PERI:(DE-600)2048329-6$$a10.1021/acs.cgd.2c01100$$gVol. 23, no. 1, p. 434 - 441$$n1$$p434 - 441$$tCrystal growth & design$$v23$$x1528-7483$$y2023
000941216 8564_ $$uhttps://juser.fz-juelich.de/record/941216/files/acs.cgd.2c01100-2.pdf
000941216 8564_ $$uhttps://juser.fz-juelich.de/record/941216/files/CGD-Fe2PW10-postprint.docx$$yPublished on 2022-12-12. Available in OpenAccess from 2023-12-12.
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