Home > Publications database > Bifunctionalized Polyoxotungstates: Dilacunary Keggin Clusters Incorporating Fe III and Organoarsonate Constituents > print

001     941216
005     20230929112507.0
024 7 _ |a 10.1021/acs.cgd.2c01100
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024 7 _ |a 2128/33786
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037 _ _ |a FZJ-2023-00820
082 _ _ |a 540
100 1 _ |a Faassen, Fabian
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245 _ _ |a Bifunctionalized Polyoxotungstates: Dilacunary Keggin Clusters Incorporating Fe III and Organoarsonate Constituents
260 _ _ |a Washington, DC
|c 2023
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520 _ _ |a Polyanions [{B-α-(OH)Fe2(PW10O37)}2{o-R–C6H4–AsO3)}2]12– (R = NH2 (1) and NO2 (2)) represent the first polyoxotungstates functionalized by both organoarsonates and FeIII. 1 and 2 comprise the rare dilacunary Keggin-type phosphotungstate {B-α-PW10O37}9– isomer that coordinates FeIII ions to form {B-α-FeIII2PW10} complexes linked into dimers via two organoarsonate groups. The title polyanions have been isolated as crystalline materials and fully characterized via single-crystal and powder X-ray diffraction, elemental analysis and IR and UV–vis spectroscopies, including solution stability studies. In addition, their electrochemical and magnetic properties have been characterized.
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700 1 _ |a Izarova, Natalya V.
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700 1 _ |a van Leusen, Jan
|0 0000-0003-3688-631X
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700 1 _ |a Kögerler, Paul
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|e Corresponding author
773 _ _ |a 10.1021/acs.cgd.2c01100
|g Vol. 23, no. 1, p. 434 - 441
|0 PERI:(DE-600)2048329-6
|n 1
|p 434 - 441
|t Crystal growth & design
|v 23
|y 2023
|x 1528-7483
856 4 _ |u https://juser.fz-juelich.de/record/941216/files/acs.cgd.2c01100-2.pdf
856 4 _ |y Published on 2022-12-12. Available in OpenAccess from 2023-12-12.
|u https://juser.fz-juelich.de/record/941216/files/CGD-Fe2PW10-postprint.docx
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