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@ARTICLE{Rosenbach:943460,
author = {Rosenbach, Carolin and Walther, Felix and Ruhl, Justine and
Hartmann, Matthias and Hendriks, Theodoor Anton and Ohno,
Saneyuki and Janek, Jürgen and Zeier, Wolfgang},
title = {{V}isualizing the {C}hemical {I}ncompatibility of {H}alide
and {S}ulfide‐{B}ased {E}lectrolytes in {S}olid‐{S}tate
{B}atteries},
journal = {Advanced energy materials},
volume = {13},
number = {6},
issn = {1614-6832},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {FZJ-2023-01031},
pages = {2203673},
year = {2023},
abstract = {Halide-based solid electrolytes are currently growing in
interest in solid-state batteries due to their high
electrochemical stability window compared to sulfide
electrolytes. However, often a bilayer separator of a
sulfide and a halide is used and it is unclear why such
setup is necessary, besides the instability of the halides
against lithium metal. It is shown that an electrolyte
bilayer improves the capacity retention as it suppresses
interfacial resistance growth monitored by impedance
spectroscopy. By using in-depth analytical characterization
of buried interphases by time-of-flight secondary ion mass
spectrometry and focused ion beam scanning electron
microscopy analyses, an indium-sulfide rich region is
detected at the halide and sulfide contact area, visualizing
the chemical incompatibility of these two electrolytes. The
results highlight the need to consider more than just the
electrochemical stability of electrolyte materials, showing
that chemical compatibility of all components may be
paramount when using halide-based solid electrolytes in
solid-state batteries.},
cin = {IEK-12},
ddc = {050},
cid = {I:(DE-Juel1)IEK-12-20141217},
pnm = {1221 - Fundamentals and Materials (POF4-122)},
pid = {G:(DE-HGF)POF4-1221},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000903650200001},
doi = {10.1002/aenm.202203673},
url = {https://juser.fz-juelich.de/record/943460},
}