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@INPROCEEDINGS{Longo:972032,
author = {Longo, Marialucia and Heigl, Raimund and Schrader, Tobias
Erich},
title = {{R}eal-time investigation of {L}ysozyme crystallization
kinetics: a neutron diffractionstudy},
reportid = {FZJ-2023-01041},
year = {2022},
abstract = {The isothermal crystallization kinetics of hen-egg-white
Lysozyme has been investigated by means of a time-resolved
neutron diffraction experiment for almost 3 days, starting
from a supersaturated solution of Lysozyme (30 mg/ml, 3 wt
$\%$ NaCl, pD 4.75 at 298 K) until the growth of crystals,
in order to have complementary information about the
crystallization kinetics1. The temporal evolution of the
intensity of the Bragg peaks, observed in the neutron
diffraction images when a single crystal appears, has been
studied. Simultaneously, the analysis of the small angle
neutron scattering curves from the Lysozyme solution, during
the crystallization process, has been performed. A
correlated behaviour between the decrease of the Lysozyme
concentration and the increase of the crystallization
fraction was observed. The crystallization kinetics was
described by means of the Johnson-Mehl-Avrami-Kolmogorov
model and parameters compatible with our previous Lysozyme
crystallization study have been found2. The Lysozyme
crystallization under constant neutron flux underlines the
known strength of neutrons in studying biological samples
without causing radiation damage.},
month = {Mar},
date = {2022-03-14},
organization = {DGK-2022: German Crystallography
Meeting, München (Germany), 14 Mar
2022 - 17 Mar 2022},
subtyp = {Other},
cin = {JCNS-FRM-II / JCNS-4 / MLZ / JCNS-1},
cid = {I:(DE-Juel1)JCNS-FRM-II-20110218 /
I:(DE-Juel1)JCNS-4-20201012 / I:(DE-588b)4597118-3 /
I:(DE-Juel1)JCNS-1-20110106},
pnm = {6G4 - Jülich Centre for Neutron Research (JCNS) (FZJ)
(POF4-6G4) / 632 - Materials – Quantum, Complex and
Functional Materials (POF4-632)},
pid = {G:(DE-HGF)POF4-6G4 / G:(DE-HGF)POF4-632},
experiment = {EXP:(DE-MLZ)BIODIFF-20140101},
typ = {PUB:(DE-HGF)24},
url = {https://juser.fz-juelich.de/record/972032},
}