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@ARTICLE{Chua:1005108,
author = {Chua, Yeong Zen and Zorn, Reiner and Schmelzer, Jürn W. P.
and Schick, Christoph and Holderer, Olaf and Zamponi,
Michaela},
title = {{D}etermination of {C}ooperativity {L}ength in a
{G}lass-{F}orming {P}olymer},
journal = {ACS physical chemistry Au},
volume = {3},
number = {2},
issn = {2694-2445},
address = {Washington, DC},
publisher = {American Chemical Society},
reportid = {FZJ-2023-01307},
pages = {172–180},
year = {2023},
abstract = {To describe the properties of glass-forming liquids, the
concepts of a cooperativity length or the size of
cooperatively rearranging regions are widely employed. Their
knowledge is of outstanding importance for the understanding
of both thermodynamic and kinetic properties of the systems
under consideration and the mechanisms of crystallization
processes. By this reason, methods of experimental
determination of this quantity are of outstanding
importance. Proceeding in this direction, we determine the
so-called cooperativity number and, based on it, the
cooperativity length by experimental measurements utilizing
AC calorimetry and quasi-elastic neutron scattering (QENS)
at comparable times. The results obtained are different in
dependence on whether temperature fluctuations in the
considered nanoscale subsystems are either accounted for or
neglected in the theoretical treatment. It is still an open
question, which of these mutually exclusive approaches is
the correct one. As shown in the present paper on the
example of poly(ethyl methacrylate) (PEMA), the cooperative
length of about 1 nm at 400 K and a characteristic time of
ca. 2 μs determined from QENS coincide most consistently
with the cooperativity length determined from AC calorimetry
measurements if the effect of temperature fluctuations is
incorporated in the description. This conclusion indicates
that─accounting for temperature fluctuations─the
characteristic length can be derived by thermodynamic
considerations from the specific parameters of the liquid at
the glass transition and that temperature does fluctuate in
small subsystems.},
cin = {JCNS-1 / IBI-8 / JCNS-4 / JCNS-FRM-II / MLZ},
ddc = {530},
cid = {I:(DE-Juel1)JCNS-1-20110106 / I:(DE-Juel1)IBI-8-20200312 /
I:(DE-Juel1)JCNS-4-20201012 /
I:(DE-Juel1)JCNS-FRM-II-20110218 / I:(DE-588b)4597118-3},
pnm = {632 - Materials – Quantum, Complex and Functional
Materials (POF4-632) / 6G4 - Jülich Centre for Neutron
Research (JCNS) (FZJ) (POF4-6G4)},
pid = {G:(DE-HGF)POF4-632 / G:(DE-HGF)POF4-6G4},
experiment = {EXP:(DE-MLZ)J-NSE-20140101 / EXP:(DE-MLZ)SPHERES-20140101},
typ = {PUB:(DE-HGF)16},
pubmed = {36968449},
UT = {WOS:001006819300001},
doi = {10.1021/acsphyschemau.2c00057},
url = {https://juser.fz-juelich.de/record/1005108},
}