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@ARTICLE{Ran:1009338,
author = {Ran, Ke and Barthel, Juri and Jin, Lei and Daesung and
Buchheit, Annika and Neuhaus, Kerstin and Baumann, Stefan
and Meulenberg, Wilhelm Albert and Mayer, Joachim},
title = {{D}irect {V}isualization of {D}istorted {T}win {B}oundaries
in {C}e-{D}oped {G}d{F}e{O}3},
journal = {Nano letters},
volume = {23},
number = {7},
issn = {1530-6984},
address = {Washington, DC},
publisher = {ACS Publ.},
reportid = {FZJ-2023-02767},
pages = {2945-2951},
year = {2023},
abstract = {Utilizing advanced transmission electron microscopy (TEM),
the structure at the (110)-type twin boundary (TB) of
Ce-doped GdFeO3 (C-GFO) has been investigated with picometer
precision. Such a TB is promising to generate local
ferroelectricity within a paraelectric system, while precise
knowledge about its structure is still largely missing. In
this work, a direct measurement of the cation off-centering
with respect to the neighboring oxygen is enabled by
integrated differential phase contrast (iDPC) imaging, and
up to 30 pm Gd off-centering is highly localized at the TB.
Further electron energy loss spectroscopy (EELS) analysis
demonstrates a slight accumulation of oxygen vacancies at
the TB, a self-balanced behavior of Ce at the Gd sites, and
a mixed occupation of Fe2+ and Fe3+ at the Fe sites. Our
results provide an informative picture with atomic details
at the TB of C-GFO, which is indispensable to further push
the potential of grain boundary engineering.},
cin = {IEK-1 / IEK-12 / ER-C-2 / ER-C-1},
ddc = {660},
cid = {I:(DE-Juel1)IEK-1-20101013 / I:(DE-Juel1)IEK-12-20141217 /
I:(DE-Juel1)ER-C-2-20170209 / I:(DE-Juel1)ER-C-1-20170209},
pnm = {1232 - Power-based Fuels and Chemicals (POF4-123) / 5351 -
Platform for Correlative, In Situ and Operando
Characterization (POF4-535) / 5353 - Understanding the
Structural and Functional Behavior of Solid State Systems
(POF4-535) / DFG project 387282673 - Die Rolle von
Grenzflächen in mehrphasigen Ceroxid-basierten Membranen
für den Einsatz in Membranreaktoren (387282673)},
pid = {G:(DE-HGF)POF4-1232 / G:(DE-HGF)POF4-5351 /
G:(DE-HGF)POF4-5353 / G:(GEPRIS)387282673},
typ = {PUB:(DE-HGF)16},
pubmed = {36972518},
UT = {WOS:000958097500001},
doi = {10.1021/acs.nanolett.3c00318},
url = {https://juser.fz-juelich.de/record/1009338},
}