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@ARTICLE{Kriegler:1017752,
author = {Kriegler, Johannes and Jaimez-Farnham, Elena and Scheller,
Maximilian and Dashjav, Enkhtsetseg and Konwitschny, Fabian
and Wach, Lovis and Hille, Lucas and Tietz, Frank and Zaeh,
Michael F.},
title = {{D}esign, production, and characterization of
three-dimensionally-structured oxide-polymer composite
cathodes for all-solid-state batteries},
journal = {Energy storage materials},
volume = {57},
issn = {2405-8289},
address = {Amsterdam},
publisher = {Elsevier},
reportid = {FZJ-2023-04288},
pages = {607 - 617},
year = {2023},
abstract = {Inorganic all-solid-state batteries with oxide electrolytes
show improved safety compared to conventional lithium-ion
batteries due to the application of a non-flammable solid
electrolyte. However, the currently applied production
methods are unsuitable for creating oxide composite cathodes
with a good interfacial contact between the solid
electrolyte and the cathode active material, which limits
the accessible discharge capacity. Thus, solid electrolyte
matrix-supported all-solid-state batteries, for which a
porous scaffold is filled with cathode active material, have
recently seen increasing research interest. This publication
introduces a scalable production route for a
matrix-supported cell concept with a
three-dimensionally-structured oxide-based composite
cathode. Directed microstructures with different geometries
were introduced into NASICON-type Li1.5Al0.5Ti1.5(PO4)3
oxide solid electrolyte layers via laser ablation. The
obtained porous scaffold was infiltrated with various
cathode slurries containing cathode active material and an
ion-conducting polymer electrolyte to fabricate hybrid
composite cathodes with an improved electrode-electrolyte
interface. Scanning electron microscopy and
energy-dispersive X-ray spectroscopy confirmed a high pore
filling degree. A promising specific discharge capacity of
120.1 mAh·g−1 was achieved during electrochemical testing
of a prototype all-solid-state battery with a
LiNi0.6Mn0.2Co0.2O2 composite cathode and a lithium metal
anode. Overall, this work serves as a proof-of-concept for
the novel, matrix-supported cell design and provides
insights into the production processes involved.},
cin = {IEK-1},
ddc = {624},
cid = {I:(DE-Juel1)IEK-1-20101013},
pnm = {1222 - Components and Cells (POF4-122) / ProFeLi -
Produktionstechnik für Festkörperbatterien mit
Lithium-Metall-Anode (13XP0184B)},
pid = {G:(DE-HGF)POF4-1222 / G:(BMBF)13XP0184B},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000952633500001},
doi = {10.1016/j.ensm.2023.03.008},
url = {https://juser.fz-juelich.de/record/1017752},
}