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@ARTICLE{Roering:1026619,
author = {Roering, Philipp and Overhoff, Gerrit Michael and Liu, Kun
Ling and Winter, Martin and Brunklaus, Gunther},
title = {{E}xternal {P}ressure in {P}olymer-{B}ased {L}ithium
{M}etal {B}atteries: {A}n {O}ften-{N}eglected {C}riterion
{W}hen {E}valuating {C}ycling {P}erformance?},
journal = {ACS applied materials $\&$ interfaces},
volume = {16},
number = {17},
issn = {1944-8244},
address = {Washington, DC},
publisher = {Soc.},
reportid = {FZJ-2024-03473},
pages = {21932 - 21942},
year = {2024},
abstract = {Solid-state batteries based on lithium metal anodes, solid
electrolytes, and composite cathodes constitute a promising
battery concept for achieving high energy density. Charge
carrier transport within the cells is governed by solid−
solid contacts, emphasizing the importance of well-designed
interfaces. A key parameter for enhancing the interfacial
contacts among electrode active materials and electrolytes
comprises externally applied pressure onto the cell stack,
particularly in the case of ceramic electrolytes. Reports
exploring the impact of external pressure on polymer-based
cells are, however, scarce due to overall better wetting
behavior. In this work, the consequences of externally
applied pressure in view of key performance indicators,
including cell longevity, rate capability, and limiting
current density in single-layer pouch-type NMC622||Li cells,
are evaluated employing cross-linked poly(ethylene oxide),
xPEO, and cross-linked cyclodextrin grafted
poly(caprolactone), xGCD-PCL. Notably, externally applied
pressure substantially changes the cell's electrochemical
cycling performance, strongly depending on the mechanical
properties of the considered polymers. Higher external
pressure potentially enhances electrode− electrolyte
interfaces, thereby boosting the rate capability of
pouch-type cells, despite the fact that the cell longevity
may be reduced upon plastic deformation of the polymer
electrolytes when passing beyond intrinsic thresholds of
compressive stress. For the softer xGCD-PCL membrane,
cycling of cells is only feasible in the absence of external
pressure, whereas in the case of xPEO, a trade-off between
enhanced rate capability and minimal membrane deformation is
achieved at cell pressures of ≤0.43 MPa, which is
considerably lower and more practical compared to cells
employing ceramic electrolytes with ≥5 MPa external
pressure.},
cin = {IEK-12},
ddc = {600},
cid = {I:(DE-Juel1)IEK-12-20141217},
pnm = {1222 - Components and Cells (POF4-122) / 1223 - Batteries
in Application (POF4-122) / FB2-POLY - Zellplattform
Polymere (BMBF-13XP0429A)},
pid = {G:(DE-HGF)POF4-1222 / G:(DE-HGF)POF4-1223 /
G:(DE-Juel1)BMBF-13XP0429A},
typ = {PUB:(DE-HGF)16},
pubmed = {38649156},
UT = {WOS:001242182900001},
doi = {10.1021/acsami.4c02095},
url = {https://juser.fz-juelich.de/record/1026619},
}