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@ARTICLE{Trapp:11850,
author = {Trapp, M. and Gutberlet, T. and Juranyi, F. and Unruh, T.
and Demé, B. and Tehei, M. and Peters, J.},
title = {{H}ydration dependent studies of highly aligned multilayer
lipid membranes by neutron scattering},
journal = {The journal of chemical physics},
volume = {133},
issn = {0021-9606},
address = {Melville, NY},
publisher = {American Institute of Physics},
reportid = {PreJuSER-11850},
pages = {164505},
year = {2010},
note = {The authors thank F. Natali and S. Busch for the fruitful
discussions. M. Trapp was supported by a Ph.D. scholarship
from the French Ministry for Research and Technology. This
research project has been supported by the European
Commission under the Sixth Framework Program through the Key
Action: Strengthening the European Research Area, Research
Infrastructures (Contract No. RII3-CT-2003-5059825). We
acknowledge the ILL and the FRM II for the allocation of
beamtime and the financial support from the Access to Major
Research Facilities Program which is a component of the
International Science Linkages Program established under the
Australian Government's innovation statement, Backing
Australia's Ability.},
abstract = {We investigated molecular motions on a picosecond timescale
of 1,2-dimyristoyl-sn-glycero-3-phosphocholine (DMPC) model
membranes as a function of hydration by using elastic and
quasielastic neutron scattering. Two different hydrations
corresponding to approximately nine and twelve water
molecules per lipid were studied, the latter being the fully
hydrated state. In our study, we focused on head group
motions by using chain deuterated lipids. Information on
in-plane and out-of-plane motions could be extracted by
using solid supported DMPC multilayers. Our studies confirm
and complete former investigations by König et al. [J.
Phys. II (France) 2, 1589 (1992)] and Rheinstädter et al.
[Phys. Rev. Lett. 101, 248106 (2008)] who described the
dynamics of lipid membranes, but did not explore the
influence of hydration on the head group dynamics as
presented here. From the elastic data, a clear shift of the
main phase transition from the P(β) ripple phase to the
L(α) liquid phase was observed. Decreasing water content
moves the transition temperature to higher temperatures. The
quasielastic data permit a closer investigation of the
different types of head group motion of the two samples. Two
different models are needed to fit the elastic incoherent
structure factor and corresponding radii were calculated.
The presented data show the strong influence hydration has
on the head group mobility of DMPC.},
keywords = {Dimyristoylphosphatidylcholine: chemistry / Membranes,
Artificial / Neutron Diffraction / Phase Transition / Water:
chemistry / Membranes, Artificial (NLM Chemicals) /
Dimyristoylphosphatidylcholine (NLM Chemicals) / Water (NLM
Chemicals) / J (WoSType)},
cin = {IFF-4 / IFF-5 / Jülich Centre for Neutron Science JCNS
(JCNS) ; JCNS},
ddc = {540},
cid = {I:(DE-Juel1)VDB784 / I:(DE-Juel1)VDB785 /
I:(DE-Juel1)JCNS-20121112},
pnm = {BioSoft: Makromolekulare Systeme und biologische
Informationsverarbeitung / Großgeräte für die Forschung
mit Photonen, Neutronen und Ionen (PNI)},
pid = {G:(DE-Juel1)FUEK505 / G:(DE-Juel1)FUEK415},
experiment = {EXP:(DE-MLZ)TOF-TOF-20140101},
shelfmark = {Physics, Atomic, Molecular $\&$ Chemical},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:21033803},
UT = {WOS:000283753600036},
doi = {10.1063/1.3495973},
url = {https://juser.fz-juelich.de/record/11850},
}