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@ARTICLE{Izarova:172042,
author = {Izarova, Natalya and Maksimovskaya, Raisa I. and Willbold,
Sabine and Kögerler, Paul},
title = {{T}etrapalladium-{C}ontaining {P}olyoxotungstate
[${P}d^{{II}}_4$(α-${P}_2{W}_{15}{O}_{56})_2$]${}^{16–}$:
{A} {C}omparative {S}tudy},
journal = {Inorganic chemistry},
volume = {53},
number = {21},
issn = {1520-510X},
address = {Washington, DC},
publisher = {American Chemical Society},
reportid = {FZJ-2014-05591},
pages = {11778–11784},
year = {2014},
abstract = {The novel tetrapalladium(II)-containing polyoxometalate
[PdII4(α-P2W15O56)2]16– has been prepared in aqueous
medium and characterized as its hydrated sodium salt
Na16[Pd4(α-P2W15O56)2]·71H2O by single-crystal XRD,
elemental analysis, IR, Raman, multinuclear NMR, and
UV–vis spectroscopy. The complex exists in anti and syn
conformations, which form in a 2:1 ratio, and possesses
unique structural characteristics in comparison with known
{M4(P2W15)2} species. 31P and 183W NMR spectroscopy are
consistent with the long-term stability of the both isomers
in aqueous solutions.},
cin = {PGI-6 / ZEA-3},
ddc = {540},
cid = {I:(DE-Juel1)PGI-6-20110106 / I:(DE-Juel1)ZEA-3-20090406},
pnm = {424 - Exploratory materials and phenomena (POF2-424)},
pid = {G:(DE-HGF)POF2-424},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000344307400048},
pubmed = {pmid:25325671},
doi = {10.1021/ic502080x},
url = {https://juser.fz-juelich.de/record/172042},
}