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000189443 1001_ $$0P:(DE-HGF)0$$aJeangros, Q.$$b0$$eCorresponding Author
000189443 245__ $$aOxidation mechanism of nickel particles studied in an environmental transmission electron microscope
000189443 260__ $$aAmsterdam [u.a.]$$bElsevier Science$$c2014
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000189443 520__ $$aThe oxidation of nickel particles was studied in situ in an environmental transmission electron microscope in 3.2 mbar of O2 between ambient temperature and 600 °C. Several different transmission electron microscopy imaging techniques, electron diffraction and electron energy-loss spectroscopy were used to study the evolution of the microstructure and the local chemical composition of the particles during oxidation. Our results suggest that built-in field effects control the initial stages of oxidation, with randomly oriented NiO crystallites and internal voids then forming as a result of outward diffusion of Ni2+ along NiO grain boundaries, self-diffusion of Ni2+ ions and vacancies, growth of NiO grains and nucleation of voids at Ni/NiO interfaces. We also observed the formation of transverse cracks in a growing NiO film in situ in the electron microscope.
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000189443 7001_ $$0P:(DE-HGF)0$$aHansen, T. W.$$b1
000189443 7001_ $$0P:(DE-HGF)0$$aWagner, J. B.$$b2
000189443 7001_ $$0P:(DE-Juel1)144121$$aDunin-Borkowski, Rafal$$b3$$ufzj
000189443 7001_ $$0P:(DE-HGF)0$$aHébert, C.$$b4
000189443 7001_ $$0P:(DE-HGF)0$$aVan herle, J.$$b5
000189443 7001_ $$0P:(DE-HGF)0$$aHessler-Wyser, A.$$b6
000189443 773__ $$0PERI:(DE-600)2014621-8$$a10.1016/j.actamat.2013.12.035$$gVol. 67, p. 362 - 372$$p362 - 372$$tActa materialia$$v67$$x1359-6454$$y2014
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