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@ARTICLE{Jeangros:189443,
author = {Jeangros, Q. and Hansen, T. W. and Wagner, J. B. and
Dunin-Borkowski, Rafal and Hébert, C. and Van herle, J. and
Hessler-Wyser, A.},
title = {{O}xidation mechanism of nickel particles studied in an
environmental transmission electron microscope},
journal = {Acta materialia},
volume = {67},
issn = {1359-6454},
address = {Amsterdam [u.a.]},
publisher = {Elsevier Science},
reportid = {FZJ-2015-02610},
pages = {362 - 372},
year = {2014},
abstract = {The oxidation of nickel particles was studied in situ in an
environmental transmission electron microscope in 3.2 mbar
of O2 between ambient temperature and 600 °C. Several
different transmission electron microscopy imaging
techniques, electron diffraction and electron energy-loss
spectroscopy were used to study the evolution of the
microstructure and the local chemical composition of the
particles during oxidation. Our results suggest that
built-in field effects control the initial stages of
oxidation, with randomly oriented NiO crystallites and
internal voids then forming as a result of outward diffusion
of Ni2+ along NiO grain boundaries, self-diffusion of Ni2+
ions and vacancies, growth of NiO grains and nucleation of
voids at Ni/NiO interfaces. We also observed the formation
of transverse cracks in a growing NiO film in situ in the
electron microscope.},
cin = {PGI-5},
ddc = {670},
cid = {I:(DE-Juel1)PGI-5-20110106},
pnm = {42G - Peter Grünberg-Centre (PG-C) (POF2-42G41)},
pid = {G:(DE-HGF)POF2-42G41},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000333495200031},
doi = {10.1016/j.actamat.2013.12.035},
url = {https://juser.fz-juelich.de/record/189443},
}