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| Hauptseite > Publikationsdatenbank > Oxidation mechanism of nickel particles studied in an environmental transmission electron microscope > print |
| Hauptseite > Publikationsdatenbank > Oxidation mechanism of nickel particles studied in an environmental transmission electron microscope > print |
| 001 | 189443 | ||
| 005 | 20240610121207.0 | ||
| 024 | 7 | _ | |a 10.1016/j.actamat.2013.12.035 |2 doi |
| 024 | 7 | _ | |a 1359-6454 |2 ISSN |
| 024 | 7 | _ | |a 1873-2453 |2 ISSN |
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| 037 | _ | _ | |a FZJ-2015-02610 |
| 082 | _ | _ | |a 670 |
| 100 | 1 | _ | |a Jeangros, Q. |0 P:(DE-HGF)0 |b 0 |e Corresponding Author |
| 245 | _ | _ | |a Oxidation mechanism of nickel particles studied in an environmental transmission electron microscope |
| 260 | _ | _ | |a Amsterdam [u.a.] |c 2014 |b Elsevier Science |
| 336 | 7 | _ | |a Journal Article |b journal |m journal |0 PUB:(DE-HGF)16 |s 1429075156_26847 |2 PUB:(DE-HGF) |
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| 336 | 7 | _ | |a article |2 DRIVER |
| 520 | _ | _ | |a The oxidation of nickel particles was studied in situ in an environmental transmission electron microscope in 3.2 mbar of O2 between ambient temperature and 600 °C. Several different transmission electron microscopy imaging techniques, electron diffraction and electron energy-loss spectroscopy were used to study the evolution of the microstructure and the local chemical composition of the particles during oxidation. Our results suggest that built-in field effects control the initial stages of oxidation, with randomly oriented NiO crystallites and internal voids then forming as a result of outward diffusion of Ni2+ along NiO grain boundaries, self-diffusion of Ni2+ ions and vacancies, growth of NiO grains and nucleation of voids at Ni/NiO interfaces. We also observed the formation of transverse cracks in a growing NiO film in situ in the electron microscope. |
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| 700 | 1 | _ | |a Hansen, T. W. |0 P:(DE-HGF)0 |b 1 |
| 700 | 1 | _ | |a Wagner, J. B. |0 P:(DE-HGF)0 |b 2 |
| 700 | 1 | _ | |a Dunin-Borkowski, Rafal |0 P:(DE-Juel1)144121 |b 3 |u fzj |
| 700 | 1 | _ | |a Hébert, C. |0 P:(DE-HGF)0 |b 4 |
| 700 | 1 | _ | |a Van herle, J. |0 P:(DE-HGF)0 |b 5 |
| 700 | 1 | _ | |a Hessler-Wyser, A. |0 P:(DE-HGF)0 |b 6 |
| 773 | _ | _ | |a 10.1016/j.actamat.2013.12.035 |g Vol. 67, p. 362 - 372 |0 PERI:(DE-600)2014621-8 |p 362 - 372 |t Acta materialia |v 67 |y 2014 |x 1359-6454 |
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