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000022279 084__ $$2WoS$$aChemistry, Inorganic & Nuclear
000022279 1001_ $$0P:(DE-HGF)0$$aFielden, J.$$b0
000022279 245__ $$aA Fluorophosphate-Based Inverse Keggin Structure
000022279 260__ $$aLondon$$bSoc.$$c2012
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000022279 500__ $$3POF3_Assignment on 2016-02-29
000022279 500__ $$aWe thank Claire Besson, Arkady Ellern and De-Liang Long for helpful discussions. Work at the Ames Laboratory (initial synthesis and structural characterization) was supported by the Department of Energy-Basic Energy Sciences under Contract No. DE-AC02-07CH11358.
000022279 520__ $$aAn unusual PFO(3)(2-)-templated "inverse Keggin" polyanion, [Mo(12)O(46)(PF)(4)](4-), has been isolated from the degradation reaction of an {Mo(132)}-type Keplerate to [PMo(12)O(40)](3-) by [Cu(MeCN)(4)](PF(6)) in acetonitrile. (31)P-NMR studies suggest a structure-directing role for [Cu(MeCN)(4)](+) in the formation of the highly unusual all-inorganic inverse Keggin structure.
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