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@ARTICLE{Radulescu:276170,
      author       = {Radulescu, Aurel and Goerigk, Günter and Fetters, Lewis
                      and Richter, Dieter},
      title        = {{M}orphology of crystalline–amorphous olefin block
                      copolymers in solution characterized by small-angle neutron
                      scattering and microscopy},
      journal      = {Journal of applied crystallography},
      volume       = {48},
      number       = {6},
      issn         = {1600-5767},
      address      = {Copenhagen},
      publisher    = {Munksgaard},
      reportid     = {FZJ-2015-06637},
      pages        = {1860-1869},
      year         = {2015},
      abstract     = {The single-chain properties and self-assembly behavior in
                      dilute solution of olefin block copolymers obtained by
                      chain-shuttling technology and consisting of alternating
                      crystallizable and amorphous ethylene/1-octene blocks were
                      investigated by pinhole and focusing small-angle neutron
                      scattering techniques, optical microscopy in bright-field
                      and crossed-polarizer modes, and differential scanning
                      calorimetry. The complex hydrocarbon soluble (precipitant
                      free) macro-aggregates formed with decreasing temperature
                      are characterized by spherulitic textures. The spherulites
                      yield, on one hand, a morphology that depends on the chain
                      structure properties and, on the other hand, multiple
                      structural levels with a hierarchical organization that
                      ranges from 10 Å up to tens of micrometres. This morphology
                      displays peculiarities dictated by the polydisperse
                      character of these materials.},
      cin          = {JCNS (München) ; Jülich Centre for Neutron Science JCNS
                      (München) ; JCNS-FRM-II / Neutronenstreuung ; JCNS-1},
      ddc          = {540},
      cid          = {I:(DE-Juel1)JCNS-FRM-II-20110218 /
                      I:(DE-Juel1)JCNS-1-20110106},
      pnm          = {144 - Controlling Collective States (POF3-144) / 6213 -
                      Materials and Processes for Energy and Transport
                      Technologies (POF3-621) / 6G15 - FRM II / MLZ (POF3-6G15) /
                      6G4 - Jülich Centre for Neutron Research (JCNS) (POF3-623)},
      pid          = {G:(DE-HGF)POF3-144 / G:(DE-HGF)POF3-6213 /
                      G:(DE-HGF)POF3-6G15 / G:(DE-HGF)POF3-6G4},
      experiment   = {EXP:(DE-MLZ)KWS2-20140101 / EXP:(DE-MLZ)KWS3-20140101},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000365774800031},
      pubmed       = {pmid:26664344},
      doi          = {10.1107/S1600576715019226},
      url          = {https://juser.fz-juelich.de/record/276170},
}