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000281764 1001_ $$0P:(DE-Juel1)129628$$aMa, Qianli$$b0$$eCorresponding author
000281764 245__ $$aA Novel Sol-Gel Method for Large-Scale Production of Nanopowders: Preparation of Li $_{1.5}$ Al $_{0.5}$ Ti $_{1.5}$ (PO $_{4}$ ) $_{3}$ as an Example
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000281764 520__ $$aSol–gel synthesis is an extensively used method for the preparation of nanopowders. However, complicated or expensive precursors, and the necessity of using organic solvent and/or heat assistance limit the method to laboratory-scaled level. An aqueous-based sol–gel method with spontaneous sol and gel formation is developed in this study. It can be applied on a large scale to synthesize compounds with Ti4+ and PO43− as major components with low cost. Al-substituted LiTi2(PO4)3 (LATP) has been widely investigated as a promising candidate for solid electrolyte in Li-ion or Li-air batteries. Major challenges such as unsatisfactory phase purity, low sintering activity, and high production costs are faced during the fabrication of LATP. In this study, as a sample application, Li1.5Al0.5Ti1.5(PO4)3 (LATP05) is conveniently prepared on a large scale by the novel sol–gel method with high phase purity, active densification behavior and high conductivity.
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000281764 7001_ $$0P:(DE-Juel1)156244$$aTsai, Chih-Long$$b2
000281764 7001_ $$0P:(DE-Juel1)129667$$aTietz, Frank$$b3
000281764 7001_ $$0P:(DE-Juel1)161591$$aGuillon, Olivier$$b4$$ufzj
000281764 773__ $$0PERI:(DE-600)2008170-4$$a10.1111/jace.13997$$gp. n/a - n/a$$n2$$p410-414$$tJournal of the American Ceramic Society$$v99$$x0002-7820$$y2016
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