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@ARTICLE{Ma:281764,
      author       = {Ma, Qianli and Xu, Qi and Tsai, Chih-Long and Tietz, Frank
                      and Guillon, Olivier},
      title        = {{A} {N}ovel {S}ol-{G}el {M}ethod for {L}arge-{S}cale
                      {P}roduction of {N}anopowders: {P}reparation of {L}i
                      $_{1.5}$ {A}l $_{0.5}$ {T}i $_{1.5}$ ({PO} $_{4}$ ) $_{3}$
                      as an {E}xample},
      journal      = {Journal of the American Ceramic Society},
      volume       = {99},
      number       = {2},
      issn         = {0002-7820},
      address      = {Oxford [u.a.]},
      publisher    = {Wiley-Blackwell},
      reportid     = {FZJ-2016-01446},
      pages        = {410-414},
      year         = {2016},
      abstract     = {Sol–gel synthesis is an extensively used method for the
                      preparation of nanopowders. However, complicated or
                      expensive precursors, and the necessity of using organic
                      solvent and/or heat assistance limit the method to
                      laboratory-scaled level. An aqueous-based sol–gel method
                      with spontaneous sol and gel formation is developed in this
                      study. It can be applied on a large scale to synthesize
                      compounds with Ti4+ and PO43− as major components with low
                      cost. Al-substituted LiTi2(PO4)3 (LATP) has been widely
                      investigated as a promising candidate for solid electrolyte
                      in Li-ion or Li-air batteries. Major challenges such as
                      unsatisfactory phase purity, low sintering activity, and
                      high production costs are faced during the fabrication of
                      LATP. In this study, as a sample application,
                      Li1.5Al0.5Ti1.5(PO4)3 (LATP05) is conveniently prepared on a
                      large scale by the novel sol–gel method with high phase
                      purity, active densification behavior and high
                      conductivity.},
      cin          = {IEK-1 / JARA-ENERGY / IEK-12},
      ddc          = {660},
      cid          = {I:(DE-Juel1)IEK-1-20101013 / $I:(DE-82)080011_20140620$ /
                      I:(DE-Juel1)IEK-12-20141217},
      pnm          = {131 - Electrochemical Storage (POF3-131)},
      pid          = {G:(DE-HGF)POF3-131},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000369836600008},
      doi          = {10.1111/jace.13997},
      url          = {https://juser.fz-juelich.de/record/281764},
}