Home > Publications database > A Novel Sol-Gel Method for Large-Scale Production of Nanopowders: Preparation of Li $_{1.5}$ Al $_{0.5}$ Ti $_{1.5}$ (PO $_{4}$ ) $_{3}$ as an Example > print

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082 _ _ |a 660
100 1 _ |a Ma, Qianli
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245 _ _ |a A Novel Sol-Gel Method for Large-Scale Production of Nanopowders: Preparation of Li $_{1.5}$ Al $_{0.5}$ Ti $_{1.5}$ (PO $_{4}$ ) $_{3}$ as an Example
260 _ _ |a Oxford [u.a.]
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|b Wiley-Blackwell
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520 _ _ |a Sol–gel synthesis is an extensively used method for the preparation of nanopowders. However, complicated or expensive precursors, and the necessity of using organic solvent and/or heat assistance limit the method to laboratory-scaled level. An aqueous-based sol–gel method with spontaneous sol and gel formation is developed in this study. It can be applied on a large scale to synthesize compounds with Ti4+ and PO43− as major components with low cost. Al-substituted LiTi2(PO4)3 (LATP) has been widely investigated as a promising candidate for solid electrolyte in Li-ion or Li-air batteries. Major challenges such as unsatisfactory phase purity, low sintering activity, and high production costs are faced during the fabrication of LATP. In this study, as a sample application, Li1.5Al0.5Ti1.5(PO4)3 (LATP05) is conveniently prepared on a large scale by the novel sol–gel method with high phase purity, active densification behavior and high conductivity.
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700 1 _ |a Xu, Qi
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700 1 _ |a Tsai, Chih-Long
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700 1 _ |a Tietz, Frank
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700 1 _ |a Guillon, Olivier
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