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000810296 1001_ $$0P:(DE-Juel1)158083$$aGuin, Marie$$b0$$eCorresponding author$$ufzj
000810296 245__ $$aNew promising NASICON material as solid electrolyte for sodium-ion batteries: Correlation between composition, crystal structure and ionic conductivity of Na$_{3+x}$Sc$_{2}$Si$_{x}$P$_{3−x}$O$_{12}$
000810296 260__ $$aAmsterdam [u.a.]$$bElsevier Science$$c2016
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000810296 520__ $$aIn the search for novel sodium-ion conductors to be used in batteries for grid application, the thoroughly studied class of NASICON materials is of great interest due to compositional diversity and high ionic conductivity. The solid solution Na3 + xSc2(SiO4)x(PO4)3 − x with 0.05 ≤ x ≤ 0.8 was investigated for the first time. The various compositions were synthesized by solid state reaction and their crystallographic and electrical properties were measured. As a result, one of the best sodium-conductive NASICON materials to date was obtained for x = 0.4 (σNa,Total = 6.9 × 10− 4 S cm− 1 at 25 °C). Furthermore, the importance of the sodium concentration and size of lattice parameters on the ionic conductivity were investigated. The bulk ionic conductivity was correlated with the structural parameters along the conduction pathway of the sodium ions and confirm the key influence of the interatomic Na–O distances on sodium ion transport.
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000810296 7001_ $$0P:(DE-Juel1)129667$$aTietz, Frank$$b1$$ufzj
000810296 7001_ $$0P:(DE-Juel1)161591$$aGuillon, Olivier$$b2$$ufzj
000810296 773__ $$0PERI:(DE-600)1500750-9$$a10.1016/j.ssi.2016.06.005$$p18-26$$tSolid state ionics$$v293$$x0167-2738$$y2016
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